Tetrahedron Letters p. 1801 - 1804 (1996)
Update date:2022-08-11
Topics:
Katagiri, Nobuya
Okada, Makoto
Kaneko, Chikara
Furuya, Toshio
New cyclic chiral nitrones constituting two diastereomers were synthesized by the reaction of isonitroso Meldrum's acid with l-menthone via a nitrosoketene intermediate. Both nitrones reacted with allyltrimelhylsilane diastereoselectively to give the corresponding isoxazolidine derivatives as sole products, which were converted to (S)- and (R)-allylglycines in ca. 100% ee, respectively.
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