Journal of the Chinese Chemical Society p. 538 - 543 (2011)
Update date:2022-07-30
Topics:
Chehardoli, Gholamabbas
Zolfigol, Mohammad Ali
Khakyzadeh, Vahid
Golbedaghi, Reza
Hall, Nikita A.
Blackman, Allan G.
The organic tribromide, [H2-cryptand 222](Br3) 2 was synthesized and characterized by X-ray crystallography, and was utilized as an active catalyst for the N-boc protection of amines. The method is general for the preparation of N-boc derivatives of aliphatic (acyclic and cyclic), aromatic, primary and secondary amines. We also applied our new reaction protocols for the N-boc protection of some new amines and spectral and physical data for the obtained products are reported.
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