Solid-liquid phase transfer catalysis without solvent coupled with microwave irradiation: A quick and efficient method for saponification of esters

Article abstract of DOI:10.1080/00397919408013814

Hindered esters can be easily saponified in a few minutes using microwave activation under solid-liquid PTC conditions without solvent. A monomode microwave reactor (Maxidigest MX 350 Prolabo) is the most efficient. A non thermal effect of microwaves is evidenced by reference to classical heating.

Full text of DOI:10.1080/00397919408013814

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Synthetic Communications: An
International Journal for Rapid
Communication of Synthetic
Organic Chemistry
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Solid-Liquid Phase Transfer
Catalysis Without Solvent
Coupled with Microwave
Irradiation: A Quick and
Efficient Method for
Saponification of Esters
André Loupy a , Philippe Pigeon a , Mohamed
Ramdani a & Patrick Jacquault b
a Laboratoire des Réactions Sélectives sur Supports,
ICMO, Université Paris-Sud, CNRS, UA 478, Bâtiment
410, 91405, ORSAY, Cedex, France
b Prolabo 12 rue Pelée, 75011, PARIS, France
Published online: 23 Sep 2006.
To cite this article: André Loupy , Philippe Pigeon , Mohamed Ramdani & Patrick
Jacquault (1994): Solid-Liquid Phase Transfer Catalysis Without Solvent Coupled with
Microwave Irradiation: A Quick and Efficient Method for Saponification of Esters,
Synthetic Communications: An International Journal for Rapid Communication of
Synthetic Organic Chemistry, 24:2, 159-165
To link to this article: http://dx.doi.org/10.1080/00397919408013814
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