Tetrahedron Asymmetry p. 2833 - 2837 (1997)
Update date:2022-08-11
Topics:
Igarashi, Yoshio
Otsutomo, Shinya
Harada, Masayuki
Nakano, Shigeru
Enzymatic resolution of indene bromohydrin acetate by hydrolysis or alcoholysis in the presence of immobilized lipase from Candida antarctica (Novozym 435) has been investigated. Enantiomerically enriched (1S,2S)-(+)-2-bromoindan-1-ol and (1R,2R)-(-)-1-acetoxy-2-bromoindan were obtained when indene bromohydrin acetate was treated with Novozym 435 and cyclohexanol in dibutyl ether for 30 hours at 40°C.
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