
Journal of the Electrochemical Society p. 1708 - 1711 (1981)
Update date:2022-08-17
Topics:
Rao
Elwell
Feigelson
Dense, well-adherent silicon was successfully deposited at minus 0. 75 plus or minus 0. 05v vs. Pt or Ag onto an inexpensive graphite substrate from the K//2SiF//6/LiK-KF molten salt system at 745 plus or minus 5 degree C. The solute concentration was in the range of 8-14 m/o. Cross-sectional views through the deposits indicate a nodular or dendritic growth up to several millimeters on top of an underlying coherent layer of 0. 2-0. 5 mm thick silicon. The polycrystalline silicon has a columnar structure with normal grain size of 250 mu m. The impurities detected were Cu, Fe, and Ni at levels less than 0. 005%. The room temperature resistivity has been found to be greater than 1 OMEGA cm.
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