2-(1-(4-chlorophenylsulfonyl)vinyl)-1,4-difluorobenzene

Base Information

Chemical Name:2-(1-(4-chlorophenylsulfonyl)vinyl)-1,4-difluorobenzene
CAS No.:471905-61-0
Molecular Formula:C14H9ClF2O2S
Molecular Weight:314.73500
Hs Code.:
Mol file:471905-61-0.mol

Synonyms:2-[[(4-chlorophenyl)sulfonyl]ethenyl]-1,4-difluorobenzene;2-[[(4-chlorophenyl)sulfonyl](cylcohexyl)methyl]-1,4-difluorobenzene;Benzene,2-[[(4-chlorophenyl)sulfonyl]cyclohexylmethyl]-1,4-difluoro;2-[1-[(4-chlorophenyl)sulfonyl]ethenyl]-1,4-difluorobenzene;2-[[(4-chlorophenyl)sulfonyl](cyclohexyl)methyl]-1,4-difluorobenzene;

Suppliers and Price of 2-(1-(4-chlorophenylsulfonyl)vinyl)-1,4-difluorobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-(1-(4-chlorophenylsulfonyl)vinyl)-1,4-difluorobenzene

Chemical Property:

PSA：42.52000
LogP:5.14360

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(1-(4-chlorophenylsulfonyl)vinyl)-1,4-difluorobenzene

There total 5 articles about 2-(1-(4-chlorophenylsulfonyl)vinyl)-1,4-difluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 470716-51-9
2-[[(4-chlorophenyl)sulfonyl]methyl]-1,4-difluorobenzene

: 51-80-9
bis-(dimethylamino)methane

: 471905-61-0
2-[1-[(4-chlorophenyl)sulfonyl]ethenyl]-1,4-difluorobenzene

Guidance literature:: With acetic anhydride; In N,N-dimethyl-formamide; at 60 ℃; for 24.5h;
DOI:10.1021/jo070407n

Reference yield:

: 470716-52-0
2-[[(4-chlorophenyl)thio]methyl]-1,4-difluorobenzene

: 471905-61-0
2-[1-[(4-chlorophenyl)sulfonyl]ethenyl]-1,4-difluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / sodium tungstate dihydrate; sulfuric acid; hydrogen peroxide / aliquat 336 / H₂O; toluene / 45 °C

2: 92 percent / acetic anhydride / dimethylformamide / 24.5 h / 60 °C

With sodium tungstate; sulfuric acid; dihydrogen peroxide; acetic anhydride; Aliquat 336; In water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo070407n

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 471905-61-0
2-[1-[(4-chlorophenyl)sulfonyl]ethenyl]-1,4-difluorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / sodium hydroxide / ethanol / cooling

2: 96 percent / sodium tungstate dihydrate; sulfuric acid; hydrogen peroxide / aliquat 336 / H₂O; toluene / 45 °C

3: 92 percent / acetic anhydride / dimethylformamide / 24.5 h / 60 °C

With sodium hydroxide; sodium tungstate; sulfuric acid; dihydrogen peroxide; acetic anhydride; Aliquat 336; In ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo070407n