N,N-Dimethyl-4-ethylaniline

Base Information

• Chemical Name: N,N-Dimethyl-4-ethylaniline
• CAS No.: 4150-37-2
• Molecular Formula: C10H15N
• Molecular Weight: 149.236
• Hs Code.: 2921420090
• DSSTox Substance ID: DTXSID10194388
• Nikkaji Number: J1.457.448D
• Wikidata: Q83067144
• Mol file: 4150-37-2.mol

Synonyms:N,N-Dimethyl-4-ethylaniline;4150-37-2;SCHEMBL44501;N,N-Dimethyl-p-ethyl-aniline;DTXSID10194388;(s)-dimethyl[1-(1-ethyl-2-phenyl)]amine

Chemical Property of N,N-Dimethyl-4-ethylaniline

Chemical Property:

• Vapor Pressure: 0.1mmHg at 25°C
• Boiling Point: 222.7°Cat760mmHg
• Flash Point: 89.2°C
• PSA: 3.24000
• Density: 0.931g/cm³
• LogP: 2.31500
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 149.120449483
• Heavy Atom Count: 11
• Complexity: 101

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1=CC=C(C=C1)N(C)C

Technology Process of N,N-Dimethyl-4-ethylaniline

There total 26 articles about N,N-Dimethyl-4-ethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

formic acid (64-18-6) + mono-N-methylaminoacetophenone (17687-47-7) → N,N-dimethyl-4-ethylaniline (4150-37-2)

Guidance literature:

With tris(pentafluorophenyl)borate; In dibutyl ether; at 100 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201503879

Reference yield: 91.0%

methanol (67-56-1) + p-aminobenzophenone (99-92-3) → N,N-dimethyl-4-ethylaniline (4150-37-2)

Guidance literature:

With 10wt%Cu-5wt%Co/γ-Al₂O₃; at 240 ℃; for 10h; Autoclave; Inert atmosphere;

Reference yield: 85.0%

4'-dimethylaminoacetophenone (2124-31-4) → N,N-dimethyl-4-ethylaniline (4150-37-2)

Guidance literature:

With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; for 10h;

DOI:10.1002/hc.20062

upstream raw materials:

N,N-dimethy-4-vinylaniline

dimethyl sulfate

4-aminoethylbenzene

4'-dimethylaminoacetophenone

Downstream raw materials:

(4-Ethyl-2-nitro-phenyl)-dimethyl-amine

C₂₆H₂₈N₂O₄S

2-(((4-ethylphenyl)(methyl)amino)methyl)cyclohexan-1-one

1-((4-ethylphenyl)(methyl)amino)-4,4-dimethylpentan-3-one