Silane, methylenebis[methyl-

Base Information

• Chemical Name: Silane, methylenebis[methyl-
• CAS No.: 5654-05-7
• Molecular Formula: C₃H₁₂Si₂
• Molecular Weight: 104.299
• DSSTox Substance ID: DTXSID10339999
• Mol file: 5654-05-7.mol

Synonyms:Silane, methylenebis[methyl-;AC1LBMVB;Silane, methylenebis*methyl-;DTXSID10339999;DSKSAXYFIBWFLQ-UHFFFAOYSA-N;Methyl[(methylsilyl)methyl]silane #

Chemical Property of Silane, methylenebis[methyl-

Chemical Property:

• Boiling Point: 71 °C(Press: 768 Torr)
• PSA: 0.00000
• LogP: -0.20400
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 100.01645332
• Heavy Atom Count: 5
• Complexity: 12.4

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si]C[Si]C

Technology Process of Silane, methylenebis[methyl-

There total 4 articles about Silane, methylenebis[methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

dichloro-1,3 dimethyl-1,3 disila-1,3 propane (26799-06-4) → bis(methylsilyl)methane (5654-05-7)

Guidance literature:

With lithium aluminium tetrahydride; In dibutyl ether; at 40 ℃; for 48h;

DOI:10.1016/0022-328X(95)00305-A

Reference yield:

polydimethylsilane → tetramethylsilane (75-76-3) + dimethylsilane (1111-74-6) + trimethylsilan (993-07-7) + 2,4-dimethyl-2,4-disilapentane (18163-84-3) + (trimethylsilylmethyl)dimethylsilane (1189-75-9) + C6H20Si3 (944573-21-1) + C7H22Si3 (944573-19-7) + C8H26Si4 + C9H28Si4 + C10H30Si4 + 2,2,4,4,6-pentamethyl-2,4,6-trisilaheptane (17905-92-9) + Dimethylsilanyl-(dimethylsilanylmethyl-dimethyl-silanyl)-methane (4180-04-5) + Bis-(dimethylsilanylmethyl-dimethyl-silanyl)-methane (18030-69-8) + bis(methylsilyl)methane (5654-05-7)

Guidance literature:

at 500 ℃; for 80.8h; under 5171.62 - 46544.6 Torr; Product distribution / selectivity;

Reference yield:

bis(trimethylsilyl)methane (2117-28-4) + trimethylsilyl(dimethylchlorosilyl)methane (13683-11-9) + bis(chlorodimethylsilyl)methane (5357-38-0,124211-70-7) + dichloro[(chlorodimethylsilyl)methyl]methylsilane (4519-04-4) + bis(methyldichlorosilyl)methane (4519-03-3) → methylsilane (992-94-9) + dimethylsilane (1111-74-6) + 2,4-dimethyl-2,4-disilapentane (18163-84-3) + (trimethylsilylmethyl)dimethylsilane (1189-75-9) + 1,3,3-Trimethyl-1,3-disilapropan (18148-13-5) + bis(methylsilyl)methane (5654-05-7)

Guidance literature:

With diethylene glycol dimethyl ether; lithium hydride; at 180 ℃; for 23h; Sealed tube;

DOI:10.1002/chem.201902722

upstream raw materials:

dichloro-1,3 dimethyl-1,3 disila-1,3 propane

dichloromethane

chloro-methyl-silane

bis(trimethylsilyl)methane

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