Silane, trimethyl(3-methyl-1-methylenebutoxy)-

Base Information

Chemical Name:Silane, trimethyl(3-methyl-1-methylenebutoxy)-
CAS No.:59417-87-7
Molecular Formula:C9H20OSi
Molecular Weight:172.343
Hs Code.:
DSSTox Substance ID:DTXSID10439185
Nikkaji Number:J764.869C
Wikidata:Q82255091

Synonyms:Silane, trimethyl(3-methyl-1-methylenebutoxy)-;59417-87-7;DTXSID10439185;2-(Trimethylsiloxy)-4-methyl-1-pentene

Suppliers and Price of Silane, trimethyl(3-methyl-1-methylenebutoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Silane, trimethyl(3-methyl-1-methylenebutoxy)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:172.128341792
Heavy Atom Count:11
Complexity:133

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CC(=C)O[Si](C)(C)C

Technology Process of Silane, trimethyl(3-methyl-1-methylenebutoxy)-

There total 1 articles about Silane, trimethyl(3-methyl-1-methylenebutoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10416-59-8
N,O-bis-(trimethylsilyl)-acetamide

: 108-10-1
4-methyl-2-pentanone

: 59417-87-7
4-methyl-2-trimethylsilyloxy-1-pentene

: 73505-43-8
((Z)-1,3-Dimethyl-but-1-enyloxy)-trimethyl-silane

: 13435-12-6
N-Trimethylsilylacetamide

Guidance literature:: With sodium; In N,N,N,N,N,N-hexamethylphosphoric triamide; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0022-328X(00)85896-9

Reference yield: 98.0%

: 59417-87-7
4-methyl-2-trimethylsilyloxy-1-pentene

: 100-52-7
benzaldehyde

: (+)-(R)-1-hydroxy-5-methyl-1-phenyl-3-hexanone

Guidance literature:: benzaldehyde; With tetrachlorosilane; bis(2,2'-diamino-1,1'-binaphthyl)-based chiral phosphoramide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -72 ℃; for 0.25h;

4-methyl-2-trimethylsilyloxy-1-pentene; In dichloromethane; at -72 ℃; for 3h;

With potassium fluoride; sodium hydrogencarbonate; In dichloromethane; water; for 8h;
DOI:10.1021/ol034641l

Reference yield: 95.0%

: 59417-87-7
4-methyl-2-trimethylsilyloxy-1-pentene

: 109-63-7
trifluoroborane diethyl ether

: 2023-48-5,28719-53-1
triphenylbismuth(V) difluoride

: (4-methyl-2-oxopentyl)triphenylbismuthonium tetrafluoroborate

Guidance literature:: In dichloromethane; under Ar; to a stirred soln. of the triarylbismuth difluoride in CH2Cl2is added BF3.Et2O at 0°C, after 1 h the silyl enol ether is added, stirred for 10 h at ambient temp.; the solvent is removed under reduced pressure, the residue is recrystd.or chromd., elem. anal.;