2-[(DIMETHYLAMINO)METHYL]-4,6-DIMETHYLBENZENOL

Base Information

• Chemical Name: 2-[(DIMETHYLAMINO)METHYL]-4,6-DIMETHYLBENZENOL
• CAS No.: 52777-93-2
• Molecular Formula: C11H17 N O
• Molecular Weight: 179.262
• Hs Code.: 2922299090
• Mol file: 52777-93-2.mol

Synonyms:Mesitol, a2-dimethylamino- (6CI);2-(Dimethylaminomethyl)-4,6-dimethylphenol; 2-(N,N-Dimethylaminomethyl)-4,6-dimethylphenol;NSC 105379; NSC 27834; a2-(Dimethylamino)mesitol

Chemical Property of 2-[(DIMETHYLAMINO)METHYL]-4,6-DIMETHYLBENZENOL

Chemical Property:

• Vapor Pressure: 0.0136mmHg at 25°C
• Boiling Point: 250.5°Cat760mmHg
• Flash Point: 95.5°C
• PSA: 23.47000
• Density: 1.012g/cm³
• LogP: 2.07060

Purity/Quality:

98%min ^*data from raw suppliers

2,4-Dimethyl-6-[(dimethylamino)methyl]phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[(DIMETHYLAMINO)METHYL]-4,6-DIMETHYLBENZENOL

There total 2 articles about 2-[(DIMETHYLAMINO)METHYL]-4,6-DIMETHYLBENZENOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + dimethyl amine (124-40-3) + 2,4-Xylenol (105-67-9) → 2-(N,N-dimethylaminomethyl)-4,6-dimethylophenol (52777-93-2)

Guidance literature:

In ethanol; for 48h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1039/c2dt30991b

Reference yield: 59.0%

bis-(dimethylamino)methane (51-80-9) + 2,4-Xylenol (105-67-9) → 2-(N,N-dimethylaminomethyl)-4,6-dimethylophenol (52777-93-2)

Guidance literature:

With sulfur dioxide; In acetonitrile; at 0 - 20 ℃; for 41h;

DOI:10.1016/S0040-4020(97)00848-X

Reference yield: 99.0%

titanium(IV) isopropylate (546-68-9) + 2-(N,N-dimethylaminomethyl)-4,6-dimethylophenol (52777-93-2) → [(2-((dimethylamino)methyl)-4,6-dimethylphenoxy)Ti(isopropoxy)3] (1394845-00-1)

Guidance literature:

In cyclohexane; at 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1039/c2dt30991b

upstream raw materials:

formaldehyd

dimethyl amine

2,4-Xylenol

bis-(dimethylamino)methane

Downstream raw materials:

2-Hydroxy-N,N,3,5-tetramethylthiobenzamid

Mesitol

2-(N,N-dimethylamino-N-oxymethyl)-4,6-dimethylophenol

6,8-dimethyl-2,2-diphenyl-1,3-benzoxathiine

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