Phenyl diethylsulfamate

Base Information

Chemical Name:Phenyl diethylsulfamate
CAS No.:1015-49-2
Molecular Formula:C10H15NO3S
Molecular Weight:229.3
Hs Code.:
DSSTox Substance ID:DTXSID20512832
Nikkaji Number:J1.629.327J
Wikidata:Q82372245
Mol file:1015-49-2.mol

Synonyms:Phenyl diethylsulfamate;1015-49-2;DTXSID20512832

Suppliers and Price of Phenyl diethylsulfamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phenyl diethylsulfamate

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:229.07726451
Heavy Atom Count:15
Complexity:261

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)S(=O)(=O)OC1=CC=CC=C1

Technology Process of Phenyl diethylsulfamate

There total 6 articles about Phenyl diethylsulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 20588-68-5
N,N-diethylsulfamoyl chloride

: 108-95-2,27073-41-2
phenol

: 1015-49-2
N,N-diethyl phenyl O-sulfamate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at -10 - 20 ℃;
DOI:10.1021/ol050393c

Reference yield:

: 1269657-62-6
3-methyl-1-(phenoxysulfonyl)-1H-imidazol-3-ium trifluoromethanesulfonate

: 109-89-7
diethylamine

: 1015-49-2
N,N-diethyl phenyl O-sulfamate

Guidance literature:: In acetonitrile;
DOI:10.1016/j.tetlet.2014.10.065

Reference yield:

: 108-95-2,27073-41-2
phenol

: 1015-49-2
N,N-diethyl phenyl O-sulfamate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / tetrahydrofuran

2: dichloromethane / 0 °C

3: acetonitrile

With caesium carbonate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2014.10.065