Bismuthonium, tetrakis(2-methoxyphenyl)-, bromide, monohydrate

Base Information

Chemical Name:Bismuthonium, tetrakis(2-methoxyphenyl)-, bromide, monohydrate
CAS No.:193490-13-0
Molecular Formula:Br*C₂₈H₂₈BiO₄*H₂O
Molecular Weight:735.428
Hs Code.:

Synonyms:

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Chemical Property of Bismuthonium, tetrakis(2-methoxyphenyl)-, bromide, monohydrate

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Technology Process of Bismuthonium, tetrakis(2-methoxyphenyl)-, bromide, monohydrate

There total 6 articles about Bismuthonium, tetrakis(2-methoxyphenyl)-, bromide, monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: tetrakis(2-methoxyphenyl)bismuthonium chloride monohydrate

: 7647-15-6
sodium bromide

: 193490-13-0
tetrakis(2-methoxyphenyl)bismuthonium bromide monohydrate

Guidance literature:: In dichloromethane; water; aq. Na-salt soln. addn. to Bi-salt soln. (CH2Cl2), mixt. stirring vigorously 30 min at room temp., org. layer sepn., aq. layer extn. (CHCl3); combined org. extracts evapn.; elem. anal.;
DOI:10.1039/a700379j

Reference yield: 39.0%

: 74-96-4
ethyl bromide

: 353-83-3
1,1,1-trifluoro-2-iodoethane

: 83724-41-8
tris(2-methoxyphenyl)bismuthine

: 193490-13-0
tetrakis(2-methoxyphenyl)bismuthonium bromide monohydrate

: tetrakis(2-methoxyphenyl)bismuthonium iodide monohydrate

Guidance literature:: With iodosylbenzene; In benzene; mixt. stirring at 40.50°C for 5 h, suspn. filtartion (Celite), filtrate evapn., residue passing through short silica gel column, residue retained on Celite bed extn. (CH2Cl2); combibed extracts evapn.;
DOI:10.1039/a700379j

Reference yield:

: 121899-81-8
tris(2-methoxyphenyl)bismuth dichloride

: 193490-13-0
tetrakis(2-methoxyphenyl)bismuthonium bromide monohydrate

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate; hexamethyldisiloxane / dichloromethane

2: dichloromethane; water

With trimethylsilyl trifluoromethanesulfonate; hexamethyldisiloxane; In dichloromethane; water;
DOI:10.1039/a700379j