1-Ethoxy-2,2,6,6-tetramethylpiperidine

Base Information

• Chemical Name: 1-Ethoxy-2,2,6,6-tetramethylpiperidine
• CAS No.: 34672-83-8
• Molecular Formula: C11H23NO
• Molecular Weight: 185.31
• DSSTox Substance ID: DTXSID90508469
• Wikidata: Q82365415
• Mol file: 34672-83-8.mol

Synonyms:1-ethoxy-2,2,6,6-tetramethylpiperidine;34672-83-8;SCHEMBL5792586;DTXSID90508469;AKOS015905062;1-ethoxy-2,2,6,6-tetramethyl-piperidine

Chemical Property of 1-Ethoxy-2,2,6,6-tetramethylpiperidine

Chemical Property:

• XLogP3: 2.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 185.177964357
• Heavy Atom Count: 13
• Complexity: 159

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCON1C(CCCC1(C)C)(C)C

Technology Process of 1-Ethoxy-2,2,6,6-tetramethylpiperidine

There total 3 articles about 1-Ethoxy-2,2,6,6-tetramethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical (2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3) → ethoxy-2,2,6,6-tetramethylpiperidine-1 (34672-83-8) + ethane (74-84-0) + ethene (74-85-1)

Guidance literature:

In toluene; at 79.85 ℃; for 1h; Further Variations:; Solvents; Temperatures; Kinetics;

DOI:10.1007/BF01430637

Reference yield:

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical (2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3) + 1-phenyl-2-(1-phenylpropylidene)hydrazine (14290-11-0) + Phenyl vinyl ketone (768-03-6,26742-84-7) → ethoxy-2,2,6,6-tetramethylpiperidine-1 (34672-83-8) + (1,3-diphenyl-1H-pyrazol-4-yl)(phenyl)methanone (7189-06-2)

Guidance literature:

With copper diacetate; In chlorobenzene; at 120 ℃; for 4h;

DOI:10.1021/acs.joc.7b01013

Reference yield:

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical (2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3) + ethyl iodide (75-03-6) + 2,6-(CH3)2C6H3NC(SiMe2Ph)2 → ethoxy-2,2,6,6-tetramethylpiperidine-1 (34672-83-8) + iodo(dimethyl)(phenyl)silane (33668-60-9) + 2,6-dimethylphenylisocyanate (28556-81-2) + 1-(dimethylphenylsilyloxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:

In benzene-d6; at 20 ℃; for 2h; Product distribution; Photolysis;

DOI:10.1021/jo991443s

upstream raw materials:

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

ethyl iodide

1-phenyl-2-(1-phenylpropylidene)hydrazine

Phenyl vinyl ketone

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