Ethylamine, N,N-dimethyl-2-(trimethylsiloxy)-

Base Information

• Chemical Name: Ethylamine, N,N-dimethyl-2-(trimethylsiloxy)-
• CAS No.: 16654-64-1
• Molecular Formula: C7H19 N O Si
• Molecular Weight: 161.319
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID70168121
• Nikkaji Number: J49.891B
• Wikidata: Q83037623
• Mol file: 16654-64-1.mol

Synonyms:ETHYLAMINE, N,N-DIMETHYL-2-(TRIMETHYLSILOXY)-;16654-64-1;(2-Dimethylaminoethoxy)trimethylsilane;BRN 2203152;N,N-dimethyl-2-trimethylsilyloxyethanamine;Silane, (2-dimethylaminoethoxy)trimethyl-;2-(Trimethylsiloxy)ethyldimethylamine;Ethanamine, N,N-dimethyl-2-[(trimethylsilyl)oxy]-;2-(Dimethylamino)ethanol, TMS derivative;SCHEMBL1535799;DTXSID70168121;trimethyl(2-dimethylaminoeth-oxy)silane;LS-68200;Dimethyl-(2-trimethylsilanyloxy-ethyl)-amine;N,N-Dimethyl-2-[(trimethylsilyl)oxy]ethanamine #

Chemical Property of Ethylamine, N,N-dimethyl-2-(trimethylsiloxy)-

Chemical Property:

• Vapor Pressure: 8.79mmHg at 25°C
• Boiling Point: 132.6°Cat760mmHg
• Flash Point: 34°C
• PSA: 12.47000
• Density: 0.833g/cm³
• LogP: 1.39950
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 161.123590764
• Heavy Atom Count: 10
• Complexity: 88.1

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)CCO[Si](C)(C)C

Technology Process of Ethylamine, N,N-dimethyl-2-(trimethylsiloxy)-

There total 2 articles about Ethylamine, N,N-dimethyl-2-(trimethylsiloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(N,N-dimethylamino)ethanol (108-01-0) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → 2-(N,N-dimethylamino)ethyl trimethylsilyl ether (16654-64-1)

Guidance literature:

With chloro-trimethyl-silane;

DOI:10.1021/jo01270a022

Reference yield:

chloro-trimethyl-silane (75-77-4) + 2-(N,N-dimethylamino)ethanol (108-01-0) → 2-(N,N-dimethylamino)ethyl trimethylsilyl ether (16654-64-1)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, 2.) 3 h, reflux;

Reference yield: 85.0%

2-(N,N-dimethylamino)ethyl trimethylsilyl ether (16654-64-1) + phenyltrifluorosilane (368-47-8) → phenyldifluoro(2-(dimethylamino)ethoxy)silane + trimethylsilyl fluoride (420-56-4)

Guidance literature:

DOI:10.1134/S0012500806080040

upstream raw materials:

2-(N,N-dimethylamino)ethanol

1,1,1,3,3,3-hexamethyl-disilazane

chloro-trimethyl-silane

Downstream raw materials:

trimethylsilyl fluoride

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