Guanidine sulfate

Base Information

• Chemical Name: Guanidine sulfate
• CAS No.: 594-14-9
• Molecular Formula: 2(CH5N3)^.H2SO4
• Molecular Weight: 353.309
• Hs Code.: 29252900
• NSC Number: 7296
• DSSTox Substance ID: DTXSID10883523
• Mol file: 594-14-9.mol

Synonyms:Chloride, Guanidinium;Chloride, Guanidium;Guanidine;Guanidine Hydrochloride;Guanidine Monohydrate;Guanidine Monohydrobromide;Guanidine Monohydrochloride;Guanidine Monohydroiodine;Guanidine Nitrate;Guanidine Phosphate;Guanidine Sulfate;Guanidine Sulfate (1:1);Guanidine Sulfate (2:1);Guanidine Sulfite (1:1);Guanidinium;Guanidinium Chloride;Guanidium Chloride;Hydrochloride, Guanidine;Monohydrate, Guanidine;Monohydrobromide, Guanidine;Monohydrochloride, Guanidine;Monohydroiodine, Guanidine;Nitrate, Guanidine;Phosphate, Guanidine;Sulfate, Guanidine

Chemical Property of Guanidine sulfate

Chemical Property:

• Appearance/Colour: White crystalline powder
• Vapor Pressure: 3.35E-05mmHg at 25°C
• Melting Point: 290-293 °C (dec.)(lit.)
• Boiling Point: 330 °C at 760 mmHg
• Flash Point: 281.6 °C
• PSA: 158.87000
• Density: 1.55g/cm3
• LogP: 0.76690
• Water Solubility.: SOLUBLE
• Hydrogen Bond Donor Count: 5
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 0
• Exact Mass: 157.01572689
• Heavy Atom Count: 9
• Complexity: 108

Purity/Quality:

99% ^*data from raw suppliers

Guanidine Sulfate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 22-24/25-36-26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(=N)(N)N.OS(=O)(=O)O

Technology Process of Guanidine sulfate

There total 15 articles about Guanidine sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

→ sulfate of 1-dioctylamino-3-guanidinopropane + guanidinium sulfate (594-14-9,1184-68-5)

Guidance literature:

Reference yield: 18.0%

bis(trimethylsilyl)sulphate (18306-29-1) + guanidine hydrochloride (50-01-1) → chloro-trimethyl-silane (75-77-4) + Hexamethyldisiloxane (107-46-0) + guanidinium sulfate (594-14-9,1184-68-5)

Guidance literature:

Heating;

Reference yield:

guanidine hydrochloride salt → guanidinium sulfate (594-14-9,1184-68-5)

Guidance literature:

With silver sulfate; In water; at 20 ℃; for 2h;

DOI:10.1039/c6ra12109h

upstream raw materials:

carbamimidoyl-amidosulfuric acid

dicyanodiamidine sulfate

phenylhydrazine

bis(trimethylsilyl)sulphate

Downstream raw materials:

2-amino-5,6-dimethyl-4(3H)-pyrimidinone

2-amino-6-methyl-4-(trifluoromethyl)pyrimidine

2-aminopyrimidine-5-carbonitrile

azobischloroformamidine

Refernces

• 1、 Huang, Haifeng,Shi, Yameng,Li, Ying,Liu, Yanfang,Yang, Jun. "Thermally stable energetic salts based on 3-nitramino-4-tetrazolefurazan". . p. 64568 - 64574. Retrieved 2016/07/21.
• 2、 Belousova,Vlasova,Voronkov. "Reaction of Bis(trimethylsilyl) Sulfate with Hexamethyldisalazane, Acetamide, and Guanidine Hydrochloride". . p. 397 - 399. Retrieved 2007/10/03.