Perovskite CH3NH3PbI3 Powder

Base Information

• Chemical Name: Perovskite CH3NH3PbI3 Powder
• CAS No.: 69507-98-8
• Molecular Formula: CH5N.H.PbI3
• Molecular Weight: 623
• Mol file: 69507-98-8.mol

Synonyms:CH3NH3PbI3;Perovskite CH3NH3PbI3 Powder;Methylammonium triiodoplumbate

Chemical Property of Perovskite CH3NH3PbI3 Powder

Chemical Property:

• PSA: 26.02000
• Density: 1.368
• LogP: 2.55150

Purity/Quality:

>99% ^*data from raw suppliers

Methylammonium triiodoplumbate(II) (40wt% solution in DMF) (99.99+%-Pb) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Perovskite CH3NH3PbI3 Powder

There total 8 articles about Perovskite CH3NH3PbI3 Powder which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methylamine hydroiodide (14965-49-2) + lead(II) iodide (10101-63-0) → methylammonium lead iodide (69507-98-8)

Guidance literature:

In N,N-dimethyl-formamide; under N2; stoich. amts.; soln. of alkylammonium salt and Pb salt in DMF at room temp.; soln. poured into nitromethane;

DOI:10.1246/bcsj.79.1607

Reference yield:

hydrogen iodide (10034-85-2) + lead(II) acetate trihydrate (6080-56-4) + methylamine (74-89-5) → methylammonium lead iodide (69507-98-8)

Guidance literature:

hydrogen iodide; lead(II) acetate trihydrate; In water; at 100 ℃; for 0.25h;

hydrogen iodide; methylamine; In water; at 75 ℃;

DOI:10.1021/acs.cgd.6b00297

Reference yield:

methylamine hydroiodide (14965-49-2) + lead acetate (301-04-2) → methylammonium lead iodide (69507-98-8)

Guidance literature:

In water; Drop-by-drop addn. of aq. soln. of Pb-compd. to excess of hot aq. soln. of org. compd. at temp. above 40°C and slow cooling to about 5°C.; Elem. anal. of obtained crystals.;

DOI:10.1016/0022-3697(90)90021-7

upstream raw materials:

hydrogen iodide

lead acetate

methylamine

methylamine hydroiodide

Refernces

• 1、 Kim, Jong H.,Kim, Sung-Hoon. "Colorimetric polarity chemosensor based on a organometal halide perovskite functional dye". . p. 73 - 78. Retrieved 2016.
• 2、 Dhanker,Brigeman,Larsen,Stewart,Asbury,Giebink. "Random lasing in organo-lead halide perovskite microcrystal networks". . . Retrieved 2014.
• 3、 Yantara, Natalia,Sabba, Dharani,Yanan, Fang,Kadro, Jeannette M.,Moehl, Thomas,Boix, Pablo P.,Mhaisalkar, Subodh,Gr?tzel, Michael,Gr?tzel, Carole. "Loading of mesoporous titania films by CH3NH3PbI3 perovskite, single step vs. sequential deposition". . p. 4603 - 4606. Retrieved 2015.
• 4、 Ye, Tao,Wang, Xizu,Li, Xianqiang,Yan, Alex Qingyu,Ramakrishna, Seeram,Xu, Jianwei. "Ultra-high Seebeck coefficient and low thermal conductivity of a centimeter-sized perovskite single crystal acquired by a modified fast growth method". . p. 1255 - 1260. Retrieved 2017/02/10.