chloroform

Base Information

• Chemical Name: chloroform
• CAS No.: 8013-54-5
• Molecular Formula: CHCl₃
• Molecular Weight: 119.378
• Mol file: 8013-54-5.mol

Synonyms:Ai3-24207;Brn 1731042;Caswell no. 192;Ccris 137;Chloroform [un1888] [poison]

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Chemical Property of chloroform

Chemical Property:

• PSA: 0.00000
• LogP: 1.98640

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of chloroform

There total 794 articles about chloroform which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,1,1,3,3,3-hexachloro-propan-2-one (116-16-5) + 2,2,2-trifluoroethanol (75-89-8) → chloroform (67-66-3,8013-54-5) + bis(2,2,2-trifluoroethyl) carbonate (1513-87-7)

Guidance literature:

With potassium fluoride; zirconium(IV) oxide; at 140 ℃; for 10h; pressure tight reactor;

Reference yield: 75.4%

trichloromethylphosphonous dichloride (3582-11-4) + butan-1-ol (71-36-3) → dibutyl hydrogen phosphite (1809-19-4) + n-Butyl chloride (109-69-3) + chloroform (67-66-3,8013-54-5)

Guidance literature:

Reference yield: 71.0%

ethanol (64-17-5) + pentachloro-2-(trimethylsiloxy)propene (87651-34-1) → chloroform (67-66-3,8013-54-5) + ethyl trimethylsilyl ether (1825-62-3) + ethyl 1,1-dichloroacetate (535-15-9)

Guidance literature:

With triethylamine; for 8h; Yields of byproduct given; Heating;

upstream raw materials:

pyridine

2-trichloromethyl-[1,3]dioxolan-2-ol

methanol

tetrachloromethane

Downstream raw materials:

1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

methyl 4,6-O-benzylidene-3-O-(p-tolylsulfonyl)-α-D-glucopyranoside

(R,S)-N-1-(phenoxy)-2-aminobutane

2,5-diethyl-piperazine