dichloro-(4-chloro-phenyl)-borane

Base Information

Chemical Name:dichloro-(4-chloro-phenyl)-borane
CAS No.:4250-46-8
Molecular Formula:C₆H₄BCl₃
Molecular Weight:193.268
Hs Code.:

Synonyms:dichloro-(4-chloro-phenyl)-borane

Suppliers and Price of dichloro-(4-chloro-phenyl)-borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of dichloro-(4-chloro-phenyl)-borane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dichloro-(4-chloro-phenyl)-borane

There total 9 articles about dichloro-(4-chloro-phenyl)-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 10294-34-5
boron trichloride

: 15799-48-1
tetra(p-chlorophenyl)tin

: 4250-46-8
dichloro-(4-chloro-phenyl)-borane

Guidance literature:: adding BCl3 to cooled (cooler with dry ice and aceton at -78 ° C)and stirred Sn(C6H4-4-Cl)4,at 0-5. degree. C rapid reaction controlled by adding dry ice, boiling 5 h under reflux; distn.;

Reference yield: 35.0%

: 10294-34-5
boron trichloride

: 108-90-7
chlorobenzene

: 19287-45-7
diborane

: 4250-46-8
dichloro-(4-chloro-phenyl)-borane

: 1333-74-0
hydrogen

: 31685-20-8
(3-chlorophenyl)dichloroborane

Guidance literature:: byproducts: boron hydride; High Pressure; under N2; diborane and trihalogen-borane was added to benzene at -130°C, then in a closed autoclave the mixture was heated to 140°C for 90 min; at -195.8°C H2 was removed, at room temp. the residue of trihalogen-borane and diborane were removed, unseparable isomers;