4-Methoxy-3-nitro-N-phenylbenzamide

Base Information

Chemical Name:4-Methoxy-3-nitro-N-phenylbenzamide
CAS No.:97-32-5
Molecular Formula:C14H12 N2 O4
Molecular Weight:272.26
Hs Code.:2924299090
European Community (EC) Number:202-572-9
NSC Number:50649
DSSTox Substance ID:DTXSID7025558
Nikkaji Number:J62.038F
Wikidata:Q81983923
ChEMBL ID:CHEMBL1325964
Mol file:97-32-5.mol

Synonyms:4-METHOXY-3-NITRO-N-PHENYLBENZAMIDE;97-32-5;3-NITRO-4-METHOXYBENZANILIDE;3-Nitro-p-anisanilide;p-Anisanilide, 3-nitro-;Benzamide, 4-methoxy-3-nitro-N-phenyl-;CCRIS 5842;EINECS 202-572-9;NSC 50649;BRN 3397509;4-Methoxy-3-nitrobenzanilide;DTXSID7025558;2-12-00-00258 (Beilstein Handbook Reference);Oprea1_224729;DTXCID205558;CHEMBL1325964;SCHEMBL19034437;4-methoxy-3-nitro-N-phenylbenzamid;NSC50649;Tox21_200743;NSC-50649;STL139190;AKOS000371586;LS-2025;CAS-97-32-5;NCGC00091837-01;NCGC00091837-02;NCGC00091837-03;NCGC00258297-01;2-BROMOPROPIONICACIDTERT-BUTYLESTER;NCI60_004220;FT-0631501;W-109365;Z27782852

Suppliers and Price of 4-Methoxy-3-nitro-N-phenylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
4-METHOXY-3-NITROBENZANILIDE Aldrich
1g
$ 168.00

American Custom Chemicals Corporation
3-NITRO-PARA-ANISANILIDE 95.00%
500G
$ 5543.83

American Custom Chemicals Corporation
3-NITRO-PARA-ANISANILIDE 95.00%
250G
$ 4972.34

American Custom Chemicals Corporation
3-NITRO-PARA-ANISANILIDE 95.00%
100G
$ 2752.09

AHH
3-Nitro-4-methoxybenzanilide 98%
100g
$ 298.00

Total 14 raw suppliers

Chemical Property of 4-Methoxy-3-nitro-N-phenylbenzamide

Chemical Property:

Appearance/Colour:light tan powder
Vapor Pressure:4.75E-06mmHg at 25°C
Refractive Index:1.6180 (estimate)
Boiling Point:382.3°Cat760mmHg
Flash Point:185°C
PSA：84.15000
Density:1.333g/cm³
LogP:3.45190
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:272.07970687
Heavy Atom Count:20
Complexity:350

Purity/Quality:

99.0% ^*data from raw suppliers

4-METHOXY-3-NITROBENZANILIDE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(=O)NC2=CC=CC=C2)[N+](=O)[O-]

Technology Process of 4-Methoxy-3-nitro-N-phenylbenzamide

There total 5 articles about 4-Methoxy-3-nitro-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.9%

: 67-56-1
methanol

: 41614-16-8
4-chloro-3-nitro-N-phenylbenzamide

: 97-32-5
3-nitro-4-methoxybenzanilide

Guidance literature:: With potassium hydroxide; for 8h; Reagent/catalyst; Reflux; Large scale; Green chemistry;

Reference yield:

: 62-53-3
aniline

: 97-32-5
3-nitro-4-methoxybenzanilide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / chlorobenzene / 2 h / 70 - 100 °C / Large scale; Green chemistry

2: potassium hydroxide / 8 h / Reflux; Large scale; Green chemistry

With thionyl chloride; potassium hydroxide; In chlorobenzene;

Reference yield:

: 96-99-1
4-chloro-3-nitrobenzoate

: 97-32-5
3-nitro-4-methoxybenzanilide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / chlorobenzene / 2 h / 70 - 100 °C / Large scale; Green chemistry

2: potassium hydroxide / 8 h / Reflux; Large scale; Green chemistry

With thionyl chloride; potassium hydroxide; In chlorobenzene;