N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide
• CAS No.: 888071-72-5
• Molecular Formula: C₁₅H₁₆N₂O₃S
• Molecular Weight: 304.37
• Mol file: 888071-72-5.mol

Synonyms:N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide

Chemical Property of N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide

There total 1 articles about N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-methoxy-benzaldehyde (123-11-5) + toluene-4-sulfonic acid hydrazide (1576-35-8) → N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide (888071-72-5)

Guidance literature:

In acetonitrile; at 20 ℃; for 2h;

DOI:10.1021/acs.joc.0c02421

Reference yield: 92.0%

benzaldehyde (100-52-7) + N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide (888071-72-5) → cis-4-methoxystilbene (1657-53-0) + E-1-(phenyl)-2-(4'-methoxyphenyl)ethene (1694-19-5)

Guidance literature:

N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide; With potassium tert-butylate; In toluene; at 0 - 20 ℃; for 1h;

benzaldehyde; With 5,10,15,20-tetraphenyl porphyrinato iron hydroxide; Aliquat 336; phosphorous acid trimethyl ester; In toluene; at 40 ℃; for 48h;

DOI:10.1021/ja029573x

Reference yield: 86.0%

N'-[(1E)-(4-methoxyphenyl)methylene]-4-methylbenzenesulfonohydrazide (888071-72-5) + tert-butyl alcohol (75-65-0) → tert-butyl p-methoxybenzyl ether (56636-80-7)

Guidance literature:

With potassium tert-butylate; for 4h; Heating;

DOI:10.1055/s-2001-18083

upstream raw materials:

4-methoxy-benzaldehyde

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

1-(4-Methoxyphenyl)pentane

1-(4-methoxyphenyl)pentanol

tert-butyl p-methoxybenzyl ether

3,5,4'-trimethoxy-trans-stilbene