2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide

Base Information

Chemical Name:2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide
CAS No.:698357-36-7
Molecular Formula:C₁₇H₁₈Cl₂N₂O₂
Molecular Weight:353.248
Hs Code.:

Synonyms:2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide

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Chemical Property of 2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide

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Technology Process of 2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide

There total 4 articles about 2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 6480-66-6
2,6-dichloro-4-methoxyaniline

: 75117-26-9
N,N-dimethyl-2-(2-vinylphenyl)acetamide

: 698357-36-7
2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide

Guidance literature:: With copper(l) iodide; copper; potassium carbonate; In toluene; for 48h; Heating;
DOI:10.1021/jm030891w

Reference yield:

: 62300-07-6
o-iodophenylacetyl chloride

: 698357-36-7
2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 0.46 g / CH₂Cl₂; H₂O / 1 h / 0 °C

2: 82 percent / K₂CO₃; CuI; Cu / toluene / 48 h / Heating

With copper(l) iodide; copper; potassium carbonate; In dichloromethane; water; toluene; 2: Ullmann coupling;
DOI:10.1021/jm030891w

Reference yield:

: 637-62-7
p-benzoquinone oxime

: 698357-36-7
2-[2-(2',6'-dichloro-4'-methoxyphenylamino)phenyl]-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / HCl (gas) / diethyl ether / 1 h / -10 - 0 °C

2: 82 percent / K₂CO₃; CuI; Cu / toluene / 48 h / Heating

With hydrogenchloride; copper(l) iodide; copper; potassium carbonate; In diethyl ether; toluene; 2: Ullmann coupling;
DOI:10.1021/jm030891w