methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate

Base Information

Chemical Name:methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate
CAS No.:808752-08-1
Molecular Formula:C₁₉H₃₀N₂O₆S
Molecular Weight:414.523
Hs Code.:

Synonyms:methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate

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Chemical Property of methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate

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Technology Process of methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate

There total 2 articles about methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.6%

: 1189-71-5
isocyanate de chlorosulfonyle

: 66399-70-0
methyl 2-(benzylamino)-4-methylpentanoate

: 75-65-0
tert-butyl alcohol

: 808752-08-1
methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate

Guidance literature:: isocyanate de chlorosulfonyle; tert-butyl alcohol; In dichloromethane; Cooling with ice;

methyl 2-(benzylamino)-4-methylpentanoate; With triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1002/jhet.136

Reference yield:

: 100-52-7
benzaldehyde

: 808752-08-1
methyl 2-(benzyl(N-(tert-butoxycarbonyl)sulfamoyl)amino)-4-methylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / acetic acid; sodium (triacetoxy)borohydride / 1,2-dichloro-ethane / 3.5 h / 20 °C

2: 66 percent / triethylamine / CH₂Cl₂ / 2.5 h / cooling

With sodium tris(acetoxy)borohydride; acetic acid; triethylamine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2004.08.044