BASIONIC(TM) AC 75

Base Information

• Chemical Name: BASIONIC(TM) AC 75
• CAS No.: 35487-17-3
• Molecular Formula: C4H6 N2 . Cl H
• Molecular Weight: 118.566
• Hs Code.: 29332900
• Mol file: 35487-17-3.mol

Synonyms:1H-Imidazole,1-methyl-, monohydrochloride (9CI); 1-Methylimidazole monohydrochloride;1-Methylimidazolium chloride; 3-Methylimidazolium chloride; N-Methylimidazolehydrochloride

Chemical Property of BASIONIC(TM) AC 75

Chemical Property:

• Vapor Pressure: 0.0499mmHg at 25°C
• Boiling Point: 231.7°C at 760 mmHg
• Flash Point: 118 °C
• PSA: 17.82000
• LogP: 1.22210

Purity/Quality:

99% ^*data from raw suppliers

1-Methylimidazolium chloride 95% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22-36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Basionic Ionic Liquids 1-Methylimidazolium chloride behaves as a solvent and catalyst during the formation of 5-hydroxymethylfurfural from fructose and sucrose via acid-catalyzed dehydration.

Technology Process of BASIONIC(TM) AC 75

There total 13 articles about BASIONIC(TM) AC 75 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-methyl-1H-imidazole (616-47-7) + 2-methoxy-ethanol (109-86-4,95507-80-5) + methanesulfonyl chloride (124-63-0) → 2-methoxyethyl methanesulfonate (16427-44-4) + 1-methylimidazolium chloride (35487-17-3)

Guidance literature:

In dichloromethane; at 10 - 20 ℃; for 4h;

Reference yield:

benzoyl chloride (98-88-4) + β-naphthol (135-19-3) → 2-naphthyl benzoate (93-44-7) + 1-methylimidazolium chloride (35487-17-3)

Guidance literature:

With 1-methyl-1H-imidazole; In dichloromethane; at 25 ℃; Kinetics; Mechanism;

Reference yield:

1-acetyl-3-methyl-1H-imidazol-3-ium chloride (28712-12-1) + 4-nitro-aniline (100-01-6,104810-17-5) → N-(4-Nitrophenyl)acetamide (104-04-1) + 1-methylimidazolium chloride (35487-17-3)

Guidance literature:

In dichloromethane; at 25 ℃; Kinetics; Mechanism;

upstream raw materials:

trifluoroethylamine

1-tosyl-3-methyl-imidazolium chloride

3-amino-5-nitro-benzoic acid methyl ester

1-acetyl-3-methyl-1H-imidazol-3-ium chloride

Downstream raw materials:

N-methylimidazolium triflate

1-methylimidazole hydrogen sulfate

1-methyl-1H-imidazole

N-Ethylimidazole

Refernces

• 1、 Monjoint, P.,Ruasse, M. F.. "Sulfonyl transfer from imidazoles". . p. 356 - 360. Retrieved 2007/10/02.
• 2、 Lapshin, S. A.,Dadali, V. A.,Litvinenko, L. M.,Simanenko, Yu. S.. "MECHANISM OF THE REACTION OF ACETYL HALIDES WITH AROMATIC AMINES IN THE PRESENCE OF N-SUBSTITUTED IMIDAZOLES". . p. 1730 - 1735. Retrieved 2007/10/02.