diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate

Base Information

• Chemical Name: diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate
• CAS No.: 107398-65-2
• Molecular Formula: C₂₅H₂₇NO₅
• Molecular Weight: 421.493

Synonyms:diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate

Chemical Property of diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate

Chemical Property:

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Technology Process of diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate

There total 4 articles about diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + ethyl 3-oxo-3-phenylpropionate (94-02-0) + methylamine (74-89-5) → diethyl 2,4-dibenzoylpentanedioate (21299-15-0) + diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate (107398-65-2)

Guidance literature:

With pyridine; In water; for 7h; Reflux;

DOI:10.1134/S1070428020100103

Reference yield: 60.0%

1,3,5-trimethyl-1,3,5-triazacyclohexane (108-74-7) + (toluene-4-sulfonyl)-acetic acid ethyl ester (2850-19-3) + ethyl 3-oxo-3-phenylpropionate (94-02-0) + ethyl 2-cyanoacetate (105-56-6) + diethyl malonate (105-53-3) → 5-cyano-5-ethoxycarbonyl-1,3-dimethyl-hexahydropyrimidine (107398-53-8) + 5,5-diethoxycarbonyl-1,3-dimethyl-hexahydropyrimidine (107398-54-9) + 1,5-dicyano-3,7-dimethyl-diazabicyclo<3,3,1>nona-2,6-dione (107398-69-6) + 5-ethoxycarbonyl-5-(4-methylphenylsulphonyl)-1,3-dimethyl-hexahydropyrimidine (107398-56-1) + 1,5-diethoxycarbonyl-3,7-dimethyl-3,7-diazabicyclo<3,3,1>nona-2,6-dione (107398-58-3) + diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate (107398-65-2)

Guidance literature:

Product distribution; Mechanism;

DOI:10.1016/S0040-4020(01)90615-5

Reference yield: 30.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + ethyl 3-oxo-3-phenylpropionate (94-02-0) + methylamine (74-89-5) → ethyl 1,3-dimethylhexahydropyrimidine-5-carboxylate (1448534-44-8) + diethyl 3-benzoyl-1-methyl-6-phenyl-1,2,3,4-tetrahydropyridine-3,5-dicarboxylate (107398-65-2)

Guidance literature:

In methanol; water; for 5h; Reflux;

DOI:10.1134/S1070428020100103

upstream raw materials:

1,3,5-trimethyl-1,3,5-triazacyclohexane

(toluene-4-sulfonyl)-acetic acid ethyl ester

ethyl 3-oxo-3-phenylpropionate

ethyl 2-cyanoacetate

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