1,4-Dioxane-2,5-diol, cis-

Base Information

• Chemical Name: 1,4-Dioxane-2,5-diol, cis-
• CAS No.: 110822-85-0
• Molecular Formula: C₄H₈O₄
• Molecular Weight: 120.105
• UNII: 1OEQ4650JR

Synonyms:Glycoaldehyde dimer, cis-;1,4-Dioxane-2,5-diol, cis-;UNII-1OEQ4650JR;1OEQ4650JR;1,4-Dioxane-2,5-diol, (2R,5R)-rel-;110822-85-0;cis-glycoaldehyde dimer;Q27252688

Chemical Property of 1,4-Dioxane-2,5-diol, cis-

Chemical Property:

• XLogP3: -1.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 120.04225873
• Heavy Atom Count: 8
• Complexity: 64.4

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1C(OCC(O1)O)O
• Isomeric SMILES: C1[C@@H](OC[C@@H](O1)O)O

Technology Process of 1,4-Dioxane-2,5-diol, cis-

There total 7 articles about 1,4-Dioxane-2,5-diol, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formamide (77287-34-4,77287-35-5,60100-09-6) → glycolaldehyde dimer (23147-58-2,110822-84-9,110822-85-0,77431-49-3) + guanazole (1455-77-2) + LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) + Oxalacetic acid (328-42-7) + succinic acid (110-15-6) + purine (120-73-0,149297-77-8,51953-03-8) + oxalic acid (144-62-7,97993-78-7) + uracil (66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6) + 2,6-diaminopyrimidin-4-ol (56-06-4) + urea (57-13-6)

Guidance literature:

With copper(II) chloride tetrahydrate; water; at 80 ℃; for 24h;

DOI:10.1002/chem.201706162

Reference yield:

formamide (77287-34-4,77287-35-5,60100-09-6) → glycolaldehyde dimer (23147-58-2,110822-84-9,110822-85-0,77431-49-3) + guanazole (1455-77-2) + parabanic acid (120-89-8) + LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) + 2-amino-1,9-dihydro-6H-purin-6-one (73-40-5) + succinic acid (110-15-6) + purine (120-73-0,149297-77-8,51953-03-8) + oxalic acid (144-62-7,97993-78-7) + guanidine nitrate (113-00-8) + 2-oxo-propionic acid (127-17-3) + urea (57-13-6) + rac-Ala-OH (302-72-7,25191-17-7,18875-37-1) + 2,4-diamino-pyrimidine-5-carboxylic acid (18588-61-9) + isocytosine (155831-93-9,176773-00-5,176799-47-6)

Guidance literature:

With water; zinc(II) chloride; at 80 ℃; for 24h;

DOI:10.1002/chem.201706162

Reference yield:

(η5-cyclopentadienyl)2(zirconium){(μ-carbonyl)molybdenum(carbonyl)2(η5-cyclopentadienyl)}{(carbonyl)(μ-η2,η1-C(methyl)2O)zirconium(methyl)(η5-cyclopentadienyl)2} + trifluoroacetic acid (76-05-1) → glycolaldehyde dimer (23147-58-2,110822-84-9,110822-85-0,77431-49-3) + 2-hydroxy-2-methylpropanal (20818-81-9)

Guidance literature:

In toluene; Treatment with CF3COOH (toluene, -30°C);

DOI:10.1021/om00100a023

upstream raw materials:

trifluoroacetic acid

formamide

Downstream raw materials:

1,2-bis(2'-hydroxyethyl)-hydrazine

2,2-dimethoxyethanol

4-Hydroxy-3,3-diphenyl-dihydro-furan-2-one

Glycolaldehyde

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