(3,3-Diethoxypropyl)diMethylaMine

Base Information

• Chemical Name: (3,3-Diethoxypropyl)diMethylaMine
• CAS No.: 16851-30-2
• Molecular Formula: C9H21NO2
• Molecular Weight: 175.26900
• Hs Code.: 2922199090
• Mol file: 16851-30-2.mol

Synonyms:1-Propanamine,3,3-diethoxy-N,N-dimethyl;N-Diethylpropylacetal-N,N'-dimethylamin;

Chemical Property of (3,3-Diethoxypropyl)diMethylaMine

Chemical Property:

• Boiling Point: 86-88 °C(Press: 15-16 Torr)
• PKA: 9.61±0.28(Predicted)
• PSA: 21.70000
• Density: 0.887±0.06 g/cm3(Predicted)
• LogP: 1.33720

Purity/Quality:

98%min ^*data from raw suppliers

(3,3-diethoxypropyl)dimethylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3,3-Diethoxypropyl)diMethylaMine

There total 4 articles about (3,3-Diethoxypropyl)diMethylaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + aminopropane diethyl acetal (41365-75-7) → β-Dimethylamino-propionaldehyd-diethylacetal (16851-30-2)

Guidance literature:

With sodium tris(acetoxy)borohydride; In dichloromethane; at 0 - 20 ℃; for 6h;

Reference yield:

methanol (67-56-1) + aminopropane diethyl acetal (41365-75-7) → 3,3-diethoxy-N-methylpropan-1-amine (56828-16-1) + β-Dimethylamino-propionaldehyd-diethylacetal (16851-30-2)

Guidance literature:

With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen; at 120 ℃; for 24h; under 15001.5 Torr; Glovebox;

DOI:10.1002/anie.201801524

Reference yield:

3-chloro-1,1-diethoxy-propane (35573-93-4) + dimethyl amine (124-40-3) → β-Dimethylamino-propionaldehyd-diethylacetal (16851-30-2)

Guidance literature:

upstream raw materials:

3-chloro-1,1-diethoxy-propane

dimethyl amine

formaldehyd

aminopropane diethyl acetal

Downstream raw materials:

N,N,N',N'-tetramethyl-1,10-diaminodecane

Refernces

• 1、 Wong et al.. "". . p. 785,787, 789. Retrieved 1974.
• 2、 -. "BENZOFURAN DERIVATIVE". Page 112-113. . Retrieved 2008/06/13.