2-Pyridinecarboxamide, N,N'-(4-methyl-1,2-phenylene)bis-

Base Information

Chemical Name:2-Pyridinecarboxamide, N,N'-(4-methyl-1,2-phenylene)bis-
CAS No.:216389-73-0
Molecular Formula:C19H16N4O2
Molecular Weight:332.362
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Pyridinecarboxamide, N,N'-(4-methyl-1,2-phenylene)bis-

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Technology Process of 2-Pyridinecarboxamide, N,N'-(4-methyl-1,2-phenylene)bis-

There total 1 articles about 2-Pyridinecarboxamide, N,N'-(4-methyl-1,2-phenylene)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-98-6
2-Picolinic acid

: 496-72-0
4-methyl-1,2-diaminobenzene

: 216389-73-0
N,N'-bis(pyridine-2-carboxamido)-4-methylbenzene

Guidance literature:: With triphenyl phosphite; In pyridine; at 50 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1002/jhet.3518

Reference yield: 95.0%

: 616-47-7
1-methyl-1H-imidazole

: 67-56-1
methanol

: 143-66-8
sodium tetraphenyl borate

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 216389-73-0
N,N'-bis(pyridine-2-carboxamido)-4-methylbenzene

: 1228178-76-4
trans-[(N,N'-bis(pyridine-2-carboxamido)-4-methylbenzene)Co(N-methylimidazole)2][BPh₄]*MeOH

Guidance literature:: With O₂; In methanol; MeOH soln. of Co compd. (0.5 mmol) added to boiling MeOH soln. of ligand(0.5 mmol), N-MeIm (0.75 mmol) added dropwise, air buubled for 3 h, fil tered, MeOH soln. of NaBPh4 (0.5 mmol) added; crystd. on storage, filtered off, washed (MeOH), dried (vac.), elem. anal.;
DOI:10.1016/j.ica.2010.01.007

Reference yield: 65.0%

: 7791-07-3
sodium perchlorate monohydrate

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 100-46-9
benzylamine

: 216389-73-0
N,N'-bis(pyridine-2-carboxamido)-4-methylbenzene

: 1071554-38-5
trans-[Co(N,N-bis(pyridine-2-carboxamido)-4-methylbenzene^(2-))(benzylamine)2]ClO₄

Guidance literature:: In methanol; to soln. Co(OAc)2*4H2O in MeOH boiling soln. ligand in MeOH was added, morpholine was added dropwise, air was bubbled through react. mixt. for 3h, soln. was filtered, soln. NaClO4*H2O in MeOH was added; ppt. was filtered, washed with EtOH-Et2O and dried in vacuo; elem. anal.;
DOI:10.1016/j.poly.2008.05.031