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Sodium perchlorate monohydrate
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Name

Sodium perchlorate monohydrate

 EINECS 231-511-9
CAS No. 7791-07-3 Density 2,02 g/cm3
PSA 83.50000 LogP 0.15000
Solubility Soluble in water. Melting Point 130 °C
Formula NaClO4.H2O Boiling Point N/A
Molecular Weight 140.456 Flash Point N/A
Transport Information UN 1502 Appearance white adhering crystals
Safety 17-26-27-36/37/39-22-13 Risk Codes 9-22-36/37/38-8
Molecular Structure Molecular Structure of 7791-07-3 (SODIUM PERCHLORATE MONOHYDRATE) Hazard Symbols OxidizingO,IrritantXi,HarmfulXn
Synonyms

Sodiumperchlorate (NaClO4) monohydrate;Sodium perchlorate monohydrate;

Article Data 8

Sodium perchlorate monohydrate Synthetic route

7601-90-3

perchloric acid

7732-18-5

water

144-55-8

sodium hydrogencarbonate

7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In perchloric acid by a react. of HClO4 with NaHCO3; evapn. to incipient crystn.;

sodium perchlorate

7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In water crystn. below 52.75°C;
In water crystn. below 52.75°C;
7601-90-3

perchloric acid

497-19-8

sodium carbonate

7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice;
In perchloric acid dissoln. of carbonate in HClO4 (72 %), repeated recrystn. (H2O);
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice, washing by dry ether, drying in vac. for 10 h at ambient temp.;
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice;
In not given neutralization, concg. to satn. concn., hot filtration, cooling the filtrate at stirring; recrystn. from water twice, washing by dry ether, drying in vac. for 10 h at ambient temp.;
497-19-8

sodium carbonate

7791-07-3

sodium perchlorate monohydrate

Conditions
ConditionsYield
With aq. HClO4 dry box.;
7791-07-3

sodium perchlorate monohydrate

88035-85-2

{(NH3)5IrOCHN(CH3)2}(3+)*3ClO4(1-)={(NH3)5IrOCHN(CH3)2}(ClO4)3

15646-83-0

{(NH3)5IrOOCH}(2+)*2ClO4(1-)={(NH3)5IrOOCH}(ClO4)2

Conditions
ConditionsYield
With sodium hydroxide In water Kinetics; stirred for 10 min at ambient temp., NaClO4*H2O was added in H2O; cooled, filtered, elem. anal.;100%
7791-07-3

sodium perchlorate monohydrate

[PdCl(η(3)-CH2C(Me)C(Me)2)]2

2-(propane-2-sulfanylmethyl)-pyridine

2-(propane-2-sulfanylmethyl)-pyridine

460720-55-2

[Pd(η3-1,1,2-Me3C3H2)(2-isopropylthiomethylpyridine)](ClO4)

Conditions
ConditionsYield
In methanol; dichloromethane stirred at room temp. under N2 for 1 h; evapd. in vacuo, residue dissolved in CH2Cl2, treated with activated charcoal, filtered through celite, filtrate was concd., treated with Et2O, ppt. was collected; elem. anal.;99%
553-26-4

4,4'-bipyridine

7791-07-3

sodium perchlorate monohydrate

563-63-3

silver(I) acetate

Ag(4,4'-bipyridine)(perchlorate)

Conditions
ConditionsYield
In water at 20℃; for 2h; Sealed tube;99%
7791-07-3

sodium perchlorate monohydrate

cis-{Pt(P(CH3)3)2(μ-OH)}2(NO3)2

di(cis-[bis(trimethylphosphane)(μ-hydroxo)platinum(II)]) nitrate

Conditions
ConditionsYield
In not given to Pt-salt NaClO4*H2O added; filtered, washed (H2O), dried in vac., elem. anal.;98%
7791-07-3

sodium perchlorate monohydrate

tetrakis(acetonitrile)palladium(II) tetrafluoroborate

C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2

75-05-8

acetonitrile

Pd(2+)*2CH3CN*2BF4(1-)*Na(1+)*ClO4(1-)*C4H3SC4H2SCHNCH2CH((OC2H4OC2H4)2O)CH2=Pd(CH3CN)2(C20H27NO5S2)(BF4)2NaClO4

Conditions
ConditionsYield
In acetonitrile equimol., a soln. of salt added to a soln. of S compd., stirred overnight at room temp.; solvent evapd., residue washed (cold diethyl ether), dried (vac.); elem.anal.;98%
7791-07-3

sodium perchlorate monohydrate

C21H24N3Pd(1+)*ClO4(1-)

603-35-0

triphenylphosphine

C39H39N3PPd(1+)*ClO4(1-)

Conditions
ConditionsYield
Stage #1: C21H24N3Pd(1+)*ClO4(1-); triphenylphosphine In dichloromethane for 0.166667h; Inert atmosphere; Schlenk technique;
Stage #2: sodium perchlorate monohydrate In dichloromethane at 20℃; for 1h; Inert atmosphere; Schlenk technique;		98%

Sodium perchlorate monohydrate Standards and Recommendations

DOT Classification:  5.1; Label: Oxidizer

Sodium perchlorate monohydrate Specification

The Sodium perchlorate monohydrate, also known as CCRIS 8893, is an inorganic substance with the formula NaClO4•H2O. It belongs to the product categories of Oxidation; Perchlorates Metal and Ceramic Science; Salts; Sodium Salts; Synthetic Reagents; ACS Grade Synthetic Reagents; Essential Chemicals; Perchlorates; Routine Reagents; HPLC; HPLC Buffer; HPLC Buffer - SolidChromatography/CE Reagents; HPLC Buffers; Solid. Its EINECS registry number is 231-511-9. With the CAS registry number 7791-07-3, its IUPAC name is sodium perchlorate hydrate. Sodium perchlorate monohydrate is used for the manufacture of perchlorate and other perchlorate, and also for the gunpowder industry.

Physical properties of Sodium perchlorate monohydrate: (1)H-Bond Donor: 1; (2)H-Bond Acceptor: 5; (3)Rotatable Bond Count: 0; (4)Exact Mass: 139.948846; (5)MonoIsotopic Mass: 139.948846; (6)Topological Polar Surface Area: 75.3; (7)Heavy Atom Count: 7; (8)Formal Charge: 0; (9)Complexity: 118; (10)Isotope Atom Count: 0; (11)Defined Atom StereoCenter Count: 0; (12)Undefined Atom StereoCenter Count: 0; (13)Defined Bond StereoCenter Count: 0; (14)Undefined Bond StereoCenter Count: 0; (15)Covalently-Bonded Unit Count: 3.

Preparation of Sodium perchlorate monohydrate: this chemical can be prepared by Na2CO3 and HClO4. Then the anhydrous sodium perchlorate was crystallized out. It can gradually absorb moisture in the air. At last, you will get Sodium perchlorate monohydrate.

When you are using this chemical, please be cautious about it as the following:
This chemical may cause inflammation to the skin or other mucous membranes. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. Whenever you will contact it, please wear suitable protective clothing, gloves and eye/face protection.

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: O.[O-]Cl(=O)(=O)=O.[Na+]
(2)InChI: InChI=1S/ClHO4.Na.H2O/c2-1(3,4)5;;/h(H,2,3,4,5);;1H2/q;+1;/p-1
(3)InChIKey: IXGNPUSUVRTQGW-UHFFFAOYSA-M

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intraperitoneal 1150mg/kg (1150mg/kg)   Journal of Agricultural and Food Chemistry. Vol. 14, Pg. 512, 1966.

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