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Basic Information
| CAS No.: | 13320-71-3 |
|---|---|
| Name: | molybdenum tetrachloride |
| Article Data: | 39 |
| Molecular Structure: | |
|
|
|
| Formula: | Cl4Mo |
| Molecular Weight: | 237.752 |
| Synonyms: | Molybdenumchloride (MoCl4) (6CI,7CI,8CI); Molybdenum tetrachloride |
| Density: | g/cm3 |
| Melting Point: | decomposes [STR93] |
| Boiling Point: | °Cat760mmHg |
| Flash Point: | °C |
| Solubility: | reacts with H2O [LID94] |
| PSA: | 0.00000 |
| LogP: | -11.98400 |
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Synthetic route
- 30411-56-4
trans-(Et2O)2MoCl4
- 13320-71-3
molybdenum(IV) chloride
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent, solid phase) MoCl4(Et2O)2 heated under vac. in oil bath at 120°C (5 h) or 130°C (2 h); elem. anal.; | 99% |
- 56-23-5
tetrachloromethane
B
- 124-38-9
carbon dioxide
C
- 201230-82-2
carbon monoxide
D
- 13320-71-3
molybdenum(IV) chloride
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent) Kinetics; byproducts: C2Cl4; heating of Mo oxides in stream of N2 with CCl4 (560 - 800 K); reaction followed by X-ray diffraction; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With oxygen at 310°C; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent) 300°C 2d, 250°C 5 d; sublimation (100°C, vac.), extraction (dry C2Cl4); |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With water In neat (no solvent) byproducts: H2, MoCl4; at 1200°C by presence of H2O;; | |
| In neat (no solvent) byproducts: H2; at 1200°C;; | |
| In neat (no solvent) byproducts: H2; at 1200°C;; | |
| With H2O In neat (no solvent) byproducts: H2, MoCl4; at 1200°C by presence of H2O;; |
- 7782-50-5
chlorine
- 7439-98-7
molybdenum
A
- 10241-05-1
molybdenum(V) chloride
B
- 13320-71-3
molybdenum(IV) chloride
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent) introduction of Cl2-gas (8-9 Torr/20 min/1.8 l/h) through purified (90min/H2 stream/1000°C) Mo powder (860 - 1160°C);; extraction of MoCl5 (CCl4); extraction MoCl4 (diethylether or water); further extraction (ethanol or water);; | A n/a B 0-10 |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| below 500 K; |
- 56-23-5
tetrachloromethane
B
- 124-38-9
carbon dioxide
C
- 201230-82-2
carbon monoxide
D
- 13320-71-3
molybdenum(IV) chloride
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent) Kinetics; byproducts: C2Cl4; heating of Mo oxide in stream of N2 with CCl4 (560 - 800 K); reaction followed by X-ray diffraction; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent) reaction on heating pulverized MoO2 with CCl4 to 250°C in a closed tube for 8h;; | 90-92 |
| High Pressure; at 250°C in an autoclave, 8 h; | 90-92 |
| In neat (no solvent) react. of MoO2 with CCl4 at 250°C;; | |
| In neat (no solvent) react. of MoO2 with CCl4 at 250°C;; | |
| In neat (no solvent) reaction on heating pulverized MoO2 with CCl4 to 250°C in a closed tube for 8h;; | 90-92 |
Conditions
| Conditions | Yield |
|---|---|
| With pyrographite mass ratio MoO2:C = 5:1; mixt. heated at 300°C in a flow of N2 loaded with CCl4; absence of moisture and oxygen; further by-product: Mo oxide chloride; removal of MoCl5 and Mo oxide chloride by vac. distn.; | A <1 B n/a |
...Expand
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molybdenum tetrachloride
