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Basic Information
| CAS No.: | 13360-63-9 |
|---|---|
| Name: | Ethylbutylamine |
| Molecular Structure: | |
|
|
|
| Formula: | C6H15 N |
| Molecular Weight: | 101.192 |
| Synonyms: | Butylamine,N-ethyl- (6CI,7CI,8CI); Butylethylamine; Ethylbutylamine; N-Butyl-N-ethylamine;N-Butylethylamine; N-Ethyl-1-butanamine; N-Ethyl-N-butylamine;N-Ethylbutanamine; N-Ethylbutylamine |
| EINECS: | 236-415-0 |
| Density: | 0.74 |
| Melting Point: | -77.8oC |
| Boiling Point: | 108 ºC |
| Flash Point: | 18 ºC |
| Solubility: | partly soluble |
| Appearance: | A colorless liquid with an ammonia-like odor. |
| Hazard Symbols: |
 
|
| Risk Codes: | R11;R22;R34 |
| Safety: | A poison by ingestion. When heated to decomposition it emits toxic vapors of NOx. |
| Transport Information: | UN 2733 |
| PSA: | 12.03000 |
| LogP: | 1.78690 |
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Synthetic route
- 13360-63-9
N-ethylbutylamine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In methanol at 20℃; for 16h; | 80% |
- 122-56-5
tributyl borane
- 81375-29-3
O-(p-toluenesulfonyl)-N-ethylhydroxylamine
- 13360-63-9
N-ethylbutylamine
Conditions
| Conditions | Yield |
|---|---|
| In tetrahydrofuran for 2h; Ambient temperature; | 77% |
- 917-54-4
methyllithium
- 33704-65-3
Butyl-phenylsulfanylmethyl-amine; hydrochloride
- 13360-63-9
N-ethylbutylamine
Conditions
| Conditions | Yield |
|---|---|
| In diethyl ether at -60℃; | 76% |
- 75-04-7
ethylamine
- 109-73-9
N-butylamine
A
- 102-82-9
tributyl-amine
B
- 13360-63-9
N-ethylbutylamine
C
- 4444-68-2
N,N-diethylbutylamine
D
- 4458-33-7
di-n-butylethylamine
E
- 111-92-2
dibutylamine
F
- 109-89-7
diethylamine
G
- 121-44-8
triethylamine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen at 200℃; under 6000.6 Torr; Reagent/catalyst; Temperature; | A n/a B 60.7% C n/a D n/a E n/a F n/a G n/a |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen at 150℃; under 3750.38 Torr; for 8h; Temperature; Pressure; Reagent/catalyst; | 55.3% |
| With hydrogen; nickel at 150℃; |
- 109-74-0
propyl cyanide
- 64-17-5
ethanol
A
- 13360-63-9
N-ethylbutylamine
B
- 4853-56-9
(butylidene)butylamine
C
- 109-73-9
N-butylamine
Conditions
| Conditions | Yield |
|---|---|
| With Co(9.8%)/SiO2 catalyst; hydrogen at 129.84℃; under 9750.98 Torr; Reagent/catalyst; Temperature; | A 30.5% B 25.6% C 42.3% |
...Expand
- 14925-83-8
N,N-dichloro-n-butylamine
- 557-20-0
diethylzinc
A
- 13360-63-9
N-ethylbutylamine
B
- 109-73-9
N-butylamine
Conditions
| Conditions | Yield |
|---|---|
| With Petroleum ether |
...Expand
- 1611-12-7
ethyl-butyliden-amine
- 13360-63-9
N-ethylbutylamine
Conditions
| Conditions | Yield |
|---|---|
| With nickel; Petroleum ether at 75℃; under 154457 Torr; Hydrogenation; | |
| With ethanol; sodium | |
| With ethanol; platinum Hydrogenation; |
- 77228-69-4
N-benzyl-N-ethylbutan-1-amine
- 13360-63-9
N-ethylbutylamine
Conditions
| Conditions | Yield |
|---|---|
| With platinum(IV) oxide; acetic acid at 65 - 75℃; Hydrogenolyse; |
Conditions
| Conditions | Yield |
|---|---|
| With ethanol; platinum Hydrogenation; | |
| (i), (ii) H2, Pd-C, EtOH; Multistep reaction; | |
| With potassium hydroxide; dipotassium hydrogenphosphate; phosphoric acid at 10 - 12℃; for 4h; electrochemical reductive amination, lead cathode, current density 0.05 A/cm2, pH 12; Yield given; |
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Ethylbutylamine
Chemistry
The molecular formula of N-ETHYLBUTYLAMINE(13360-63-9) is C6H15N and its formula weight is 101.19g/mol.Its EINECS is 236-415-0.Its liansport information is UN 2733.The appearance of N-ETHYLBUTYLAMINE(13360-63-9) is colorless liquid.The density of ) is 0.74 g/mL at 25 °C(lit.).The boiling point is 108 °C(lit.).The refractive index is about n20/D 1.405(lit.) and molar refractivity is 33.44 cm3.Its fiash point is 18.3 °C and the vapor pressenge is 18 mm Hg ( 20 °C).Its enthalpy of vaporization is 33.97 kJ/mol.Surface Tension is 23 dyne/cm.N-ETHYLBUTYLAMINE(13360-63-90) has the property of being soluble in alcohol, ether and other organic solvents,partly dissolved in water.
The chemical synonyms of are 1-Butanamine,N-ethyl-;butyl(ethyl)amine;Butylamine, N-ethyl-;Butylamine,N-ethyl-;Butylethylamine;N-Butylethylamine;N-Butyl-N-ethylamine;n-ethyl-1-butanamin .Its product categories is Amines;C2 to C6 and Nitrogen Compounds.The molecular structure of N-ETHYLBUTYLAMINE(13360-63-9) is
.
The chemical synonyms of are 1-Butanamine,N-ethyl-;butyl(ethyl)amine;Butylamine, N-ethyl-;Butylamine,N-ethyl-;Butylethylamine;N-Butylethylamine;N-Butyl-N-ethylamine;n-ethyl-1-butanamin .Its product categories is Amines;C2 to C6 and Nitrogen Compounds.The molecular structure of N-ETHYLBUTYLAMINE(13360-63-9) is
.Uses
N-ETHYLBUTYLAMINE(13360-63-9) can be used as intermediate of herbicide .
Production
Its preparation method is that alcohol and ammonia react with ethanol in the deoxidation and the presence of hydrogenation catalyst in the 170 ~ 210 ℃ / 1013 kPa , at the same time aminating and aminating derived products.
Toxicity Data With Reference
| 1. | orl-rat LD50:310 mg/kg | GISAAA Gigiena i Sanitariya. 39 (3)(1974),106. | ||
| 2. | orl-mus LD50:418 mg/kg | GISAAA Gigiena i Sanitariya. 39 (3)(1974),106. |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
A poison by ingestion. When heated to decomposition it emits toxic vapors of NOx. Risk Codes:R11;R22;R34
Hazard codes is 
F, 
C .
Risk statements is 11-22-34 and safety statements is 16-26-36/37/39-45-33.
HazardClass is 3.