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| CAS No.: | 134-83-8 |
|---|---|
| Name: | 4-Chlorobenzhydrylchloride |
| Molecular Structure: | |
|
|
|
| Formula: | C13H10Cl2 |
| Molecular Weight: | 237.128 |
| Synonyms: | Methane,chloro(p-chlorophenyl)phenyl- (6CI,7CI,8CI);4-Chlorobenzhydryl chloride;Chloro(p-chlorophenyl)phenylmethane;NSC 49126;p-Chlorobenzhydryl chloride;Chloro(4-chlorophenyl)phenylmethane; |
| EINECS: | 205-158-6 |
| Density: | 1.23 g/cm3 |
| Boiling Point: | 352.7 °C at 760 mmHg |
| Flash Point: | 146.9 °C |
| Solubility: | immiscible with water |
| Appearance: | colorless or Off-yellow liquid |
| Hazard Symbols: |
 C
|
| Risk Codes: | 34-36/37-36 |
| Safety: | 26-27-36/37/39-45 |
| Transport Information: | UN 3265 8/PG 2 |
| PSA: | 0.00000 |
| LogP: | 4.66820 |
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| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethanol Heating; | 95% |
| With hydrogenchloride; diethyl ether | |
| With hydrogenchloride; benzene |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 90 percent / sodium borohydride 2: 95 percent / hydrochloric acid / ethanol / Heating View Scheme | |
| Multi-step reaction with 2 steps 1: NaBH4 / tetrahydrofuran 2: HCl, CaCl2 / benzene View Scheme | |
| Multi-step reaction with 2 steps 1: NaBH4 / propan-2-ol 2: HCl, Drierite / CH2Cl2 View Scheme |
| Conditions | Yield |
|---|---|
| With N-chloro-succinimide; 9-(2-mesityl)-10-methylacridinium perchlorate In dichloromethane at 20℃; for 1h; Sealed tube; Inert atmosphere; Irradiation; |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: tetrahydrofuran / 1 h / 20 °C 2: SOCl2 / CH2Cl2 / 1 h / 0 °C View Scheme |
- 134-83-8
1-chloro-4-(chloro(phenyl)methyl)benzene
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: tetrahydrofuran / 1 h / 20 °C 2: SOCl2 / CH2Cl2 / 1 h / 0 °C View Scheme |
- 7647-01-0
hydrogenchloride
- 119-56-2
(4-chlorophenyl)phenylmethanol
- 71-43-2
benzene
A
- 134-83-8
1-chloro-4-(chloro(phenyl)methyl)benzene
B
- 7732-18-5
water
| Conditions | Yield |
|---|---|
| at 60℃; Equilibrium constant; |
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; water In chloroform for 3h; Time; Reflux; | 97% |
- 120-43-4
4-ethoxycarbonylpiperazine
- 134-83-8
1-chloro-4-(chloro(phenyl)methyl)benzene
- 80476-89-7
ethyl {4-[(4-chlorophenyl)phenylmethyl]piperazin-1-yl}carboxylate
| Conditions | Yield |
|---|---|
| With potassium carbonate In acetonitrile at 20℃; for 24h; | 96% |
| Conditions | Yield |
|---|---|
| With trifluorormethanesulfonic acid at 130℃; for 1.5h; | A n/a B 91% |
- 134-83-8
1-chloro-4-(chloro(phenyl)methyl)benzene
- 603-35-0
triphenylphosphine
- 25361-60-8
<(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride
| Conditions | Yield |
|---|---|
| at 160℃; for 6h; | 88% |
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Chemistry
Product Name: 4-Chlorobenzhydrylchloride (CAS NO.134-83-8)
Molecular Formula: C13H10Cl2
Molecular Weight: 237.13g/mol
Mol File: 134-83-8.mol
EINECS: 205-158-6
Appearance: clear light yellow liquid
Boiling point: 319.6 °C at 760 mmHg
Flash Point: 139.8 °C
Density: 1.23 g/cm3
Refractive index: n20/D 1.603(lit.)
Water Solubility: IMMISCIBLE
Sensitive: Moisture Sensitive
Index of Refraction: 1.593
Molar Refractivity: 65.35 cm3
Molar Volume: 192.7 cm3
Surface Tension: 41.7 dyne/cm
Enthalpy of Vaporization: 53.89 kJ/mol
Vapour Pressure: 0.000626 mmHg at 25°C
XLogP3-AA: 5.1
H-Bond Donor: 0
H-Bond Acceptor: 0
Structure Descriptors of 4-Chlorobenzhydrylchloride (CAS NO.134-83-8):
IUPAC Name: 1-chloro-4-[chloro(phenyl)methyl]benzene
Canonical SMILES: C1=CC=C(C=C1)C(C2=CC=C(C=C2)Cl)Cl
InChI: InChI=1S/C13H10Cl2/c14-12-8-6-11(7-9-12)13(15)10-4-2-1-3-5-10/h1-9,13H
InChIKey: ALKWTKGPKKAZMN-UHFFFAOYSA-N
Safety Profile
Safety Information of 4-Chlorobenzhydrylchloride (CAS NO.134-83-8):
Hazard Codes: C
Risk Statements: 34-36/37-36
R34:Causes burns.
R36/37:Irritating to eyes and respiratory system.
R36:Irritating to eyes.
Safety Statements: 26-27-36/37/39-45
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S27:Take off immediately all contaminated clothing.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
S45:In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: UN 3265 8/PG 2
WGK Germany: 3
HazardClass: 8
PackingGroup: II
HS Code: 29036990
Specification
4-Chlorobenzhydrylchloride , its CAS NO. is 134-83-8, the synonyms are Chloro(p-chlorophenyl)phenylmethane ; Benzene, 1-chloro-4-(chlorophenylmethyl)- ; Methane, chloro(p-chlorophenyl)phenyl- (8CI) ; alpha,4-Dichloro-alpha-phenyltoluene .