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25952-53-8

Basic Information
CAS No.: 25952-53-8
Name: 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride
Article Data: 4
Molecular Structure:
Molecular Structure of 25952-53-8 (1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride)
Formula: C8H18ClN3
Molecular Weight: 191.704
Synonyms: 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride;
EINECS: 247-361-2
Density: 0.877g/mLat 20°C(lit.)
Melting Point: 110-115 °C(lit.)
Boiling Point: 197.7 °C at 760 mmHg
Flash Point: 73.4 °C
Solubility: Soluble in water
Appearance: White crystalline powder
Hazard Symbols: CorrosiveC, IrritantXi
Risk Codes: 34-36/37/38-41-37/38-20/21/22
Safety: 26-36/37/39-45-37/39-36
Transport Information: UN 2735 8/PG 3
PSA: 27.96000
LogP: 1.93390
Synthetic route
1892-57-5

N-(3-dimethylaminopropyl)-N-ethylcarbodiimide

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

Conditions
ConditionsYield
With triethylamine hydrochloride In acetonitrile at 15℃; for 1h; Temperature;92%

{7-cyano-2-[4-(4-fluorophenyl)-1-piperazinyl]-3-[3-(trifluoromethyl)phenyl]-3,4-dihydro-4-quinazolinyl}-acetic acid methyl ester

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

Conditions
ConditionsYield
With hydrogenchloride at 90℃; for 42h;66%
628-13-7

pyridine hydrochloride

1892-57-5

N-(3-dimethylaminopropyl)-N-ethylcarbodiimide

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

Conditions
ConditionsYield
In dichloromethane at 30℃; Solvent; Temperature;71.2 g
18997-72-3

N-(3-Dimethylamino-propyl)-dithiocarbamidsaeure

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: chloroformic acid ethyl ester; triethylamine / dichloromethane / 3 h / 10 - 15 °C
2: dichloromethane / 1 h / 10 - 15 °C
3: sodium hypochlorite; ethylenediaminetetraacetic acid / 30 °C
4: dichloromethane / 30 °C
View Scheme
27421-70-1

3-(dimethylamino)propyl isothiocyanate

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dichloromethane / 1 h / 10 - 15 °C
2: sodium hypochlorite; ethylenediaminetetraacetic acid / 30 °C
3: dichloromethane / 30 °C
View Scheme
109-55-7

1-amino-3-(dimethylamino)propane

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: methanol / 2 h / 10 - 20 °C
2: chloroformic acid ethyl ester; triethylamine / dichloromethane / 3 h / 10 - 15 °C
3: dichloromethane / 1 h / 10 - 15 °C
4: sodium hypochlorite; ethylenediaminetetraacetic acid / 30 °C
5: dichloromethane / 30 °C
View Scheme
735265-93-7

5-(4-Methoxyphenyl)-4-(6-methoxy-3-pyridinyl)-1,3-oxazole-2-carboxylic acid

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

5-(4-Methoxyphenyl)-4-(6-methoxy-3-pyridinyl)-1,3-oxazole-2-carboxamide

Conditions
ConditionsYield
With benzotriazol-1-ol In DMF (N,N-dimethyl-formamide) at 0℃; for 18h;100%
24057-28-1

pyridinium p-toluenesulfonate

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

1363481-45-1

EDCI*TsOH

Conditions
ConditionsYield
With potassium carbonate In dichloromethane100%
25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride

Conditions
ConditionsYield
With water at 20℃;100%
5680-79-5

glycine ethyl ester hydrochloride

25952-53-8

1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

1205-08-9

methyl hippurate

Conditions
ConditionsYield
With sodium hydrogencarbonate; benzotriazol-1-ol; benzoic acid98%
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    Name: 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride Synonyms: 1-Ethyl-3-(3-dimethylaminopropyl) carbodiimide Hydrochloride CAS: 25952-53-8 MF: C7H18ClN3 Appearance:White powder Storage:Store in cool and dry place, away from sun light

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  • 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride  CAS No 25952-53-8

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  • 1-ETHYL-3-(3-DIMETHYLAMINOPROPYL) CARBODIIMIDE 25952-53-8

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    25952-53-8

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    Synonyms: (3-dimethylaminopropyl)ethyl-carbodiimidmonohydrochloride;3-propanediamine,n’-(ethylcarbonimidoyl)-n,n-dimethyl-monohydrochloride;edap;edc(reagent);WSCD;WSCI;WATER-SOLUBLE CARBODIIMIDE;1-ETHYL-3-(3-DIMETHYLAMINOPROPYL) CARBODIIMIDE

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  • Enought Inventory1-Ethyl-3-(dimethylaminopropyl) carbodiimide hydrochloride

  • Casno:

    25952-53-8

    Enought Inventory1-Ethyl-3-(dimethylaminopropyl) carbodiimide hydrochloride

    Min.Order: 3000 Kilogram

    FOB Price:  USD $ 30.0-50.0

    Located in Wuhan City of Hubei Province, Wuhan Rison Trading co., Ltd is engaged in the supply of fine specialty chemicals. Our business includes metal surface treatment, such as nickel/zinc/copper plating, perfluoro chemicals, tin salts (stannous su

    Founded in 2005, Hubei Rison Chemical Co. Ltd, is specializing in the development, production and marketing of speciality chemicals. We have our own chemical factory, which is ma

  •  HUBEI RISON CHEMICAL CO.,LTD.

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    Tel:0086-27-83607103/83642615

    Address:No.498, Jianshe Ave, Wuhan, China

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  • 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride

  • Casno:

    25952-53-8

    1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 80.0-100.0

    About us Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad.

    Baoji Guokang Healthchem co.,ltd located in Baoji High-tech Zone,is epitomizing international,cooperative and honest.We are a young company full of action and energy,and our profes

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    Address:China

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  • CAS NO.:25952-53-8

  • Casno:

    25952-53-8

    CAS NO.:25952-53-8

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

    The company is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds,

  •  Henan Wentao Chemical Product Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-370-2722992

    Address:32 Room, 5th Floor, Building 11, No. 6 Yinxing Road, High-tech Industrial Development Zone, Zhengzhou City, Henan Province

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Consensus Reports

Reported in EPA TSCA Inventory.

Specification

The 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride is an organic compound with the formula C8H18ClN3. The IUPAC name of this chemical is 3-(ethyliminomethylideneamino)-N,N-dimethylpropan-1-amine hydrochloride. With the CAS registry number 25952-53-8, it is also named as 1-Ethyl-3-(3-dimethylaminopropyl)carbodiimide monohydrochloride. The product's categories are Straight Chain Compounds; Aliphatics; Peptide Coupling Reagents; Biochemistry; Condensation & Active Esterification; Coupling Reactions (Peptide Synthesis); Peptide Synthesis; Reagents for Oligosaccharide Synthesis; Synthetic Organic Chemistry; Peptide; Amine. Besides, it is a white crystalline powder, which should be stored at temperature of -20 °C. It is mainly used as dehydrating agent of peptides, proteins and nucleotide synthesis.

Physical properties of 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride:
(1)ACD/LogP: 2.32; (2)ACD/LogD (pH 5.5): -0.73; (3)ACD/LogD (pH 7.4): 0.25; (4)ACD/BCF (pH 5.5): 1; (5)ACD/BCF (pH 7.4): 1; (6)ACD/KOC (pH 5.5): 1; (7)ACD/KOC (pH 7.4): 3.67; (8)#H bond acceptors: 3; (9)#Freely Rotating Bonds: 5; (10)Polar Surface Area: 27.96 Å2; (11)Flash Point: 73.4 °C; (12)Enthalpy of Vaporization: 43.39 kJ/mol; (13)Boiling Point: 197.7 °C at 760 mmHg; (14)Vapour Pressure: 0.373 mmHg at 25°C.

Structure descriptors of 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride
(1)SMILES: Cl.N(=C=N\CCCN(C)C)\CC
(2)InChI: InChI=1/C8H17N3.ClH/c1-4-9-8-10-6-5-7-11(2)3;/h4-7H2,1-3H3;1H
(3)InChIKey: FPQQSJJWHUJYPU-UHFFFAOYAS
(4)Std. InChI: InChI=1S/C8H17N3.ClH/c1-4-9-8-10-6-5-7-11(2)3;/h4-7H2,1-3H3;1H
(5)Std. InChIKey: FPQQSJJWHUJYPU-UHFFFAOYSA-N

Uses of 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride:
1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride can be used to produce (17R)-2'-ethylimino-3'-dimethylaminopropylspiro(androst-4-ene-17,5'-oxazolidine)-3,4'-dione at ambient temperature. It will need reagent solvent dimethylformamide with reaction time of 3 hours. The yield is about 31%.


Safety information of 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride:
It is harmful by inhalation, in contact with skin and if swallowed and can cause burns. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. Besides, this chemical is irritating to eyes, respiratory system and skin and risk of serious damage to eyes. When you are using it, wear suitable gloves and eye/face protection. In case of accident or if you feel unwell seek medical advice immediately (show the label where possible).

The toxicity data of
1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intravenous 56mg/kg (56mg/kg)   U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#03375,