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274901-16-5

Basic Information
CAS No.: 274901-16-5
Name: 2-Pyrrolidinecarbonitrile,1-[2-[(3-hydroxytricyclo[3.3.1.13,7]dec-1-yl)amino]acetyl]-, (2S)-
Article Data: 40
Cas Database
Molecular Structure:
Molecular Structure of 274901-16-5 (2-Pyrrolidinecarbonitrile,1-[2-[(3-hydroxytricyclo[3.3.1.13,7]dec-1-yl)amino]acetyl]-, (2S)-)
Formula: C17H25N3O2
Molecular Weight: 303.404
Synonyms: 2-Pyrrolidinecarbonitrile,1-[[(3-hydroxytricyclo[3.3.1.13,7]dec-1-yl)amino]acetyl]-, (2S)- (9CI);Galvus;LAF 237;NVP-LAF 237;(-)-(2s)-1-(((3-hydroxytricyclo(3.3.1.1(3,7))dec-1-yl)amino)acetyl)pyrrolidine-2-carbonitrile;
EINECS: 630-410-0
Density: 1.27 g/cm3
Melting Point: 153-155?C
Boiling Point: 531.3 °C at 760 mmHg
Flash Point: 275.1 °C
Solubility: N/A
Appearance: white crystalline powder
Hazard Symbols: N/A
Risk Codes: 28-38-41-48
Safety: 24/25-26-28-36/37/39
Transport Information: N/A
PSA: 76.36000
LogP: 1.50308
Synthetic route

1-[2-(3-hydroxyadamant-1-yl-amino)acetyl]pyrrolidin-(2S)-carbonitrile calcium(II)-chloride

274901-16-5

vildagliptin

Conditions
ConditionsYield
With sodium carbonate; sodium chloride In dichloromethane at 20 - 40℃; Product distribution / selectivity;95%
With sodium carbonate In water at 40℃; for 0.0333333h; Product distribution / selectivity;75%

(2S)‐1‐[[(3-hydroxytricyclo[3.3.1.1[3,7]]decane-1-yl)imino]acetyl]pyrrolidine-2-carbonitrile

274901-16-5

vildagliptin

Conditions
ConditionsYield
With palladium on activated charcoal; ammonium formate In tetrahydrofuran at 20℃; for 8h; Reagent/catalyst; Solvent; Temperature;91.9%
With palladium on activated charcoal; ammonium formate In tetrahydrofuran at 20℃; for 10h; Solvent; Reagent/catalyst; Temperature;91.9%
1032564-18-3

(3-hydroxyadamantan-1-ylamino)acetic acid

(S)-pyrrolidine-2-carbonitrile p-toluenesulfonate

274901-16-5

vildagliptin

Conditions
ConditionsYield
Stage #1: C12H14N2O3S With sodium hydroxide In dichloromethane at 0℃; for 1.5h;
Stage #2: (3-hydroxyadamantan-1-ylamino)acetic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 0℃; Concentration;
90.8%

C16H33NOSi2

207557-35-5

(S)-1-(2-chloroacetyl)pyrrolidine-2-carbonitrile

274901-16-5

vildagliptin

Conditions
ConditionsYield
Stage #1: C16H33NOSi2; (S)-1-(2-chloroacetyl)pyrrolidine-2-carbonitrile With N-ethyl-N,N-diisopropylamine; potassium iodide In acetonitrile at 75 - 80℃; for 3h;
Stage #2: With ethanol In acetonitrile for 2h; Reagent/catalyst;
88.3%
702-82-9

3-aminoadamantan-1-ol

207557-35-5

(S)-1-(2-chloroacetyl)pyrrolidine-2-carbonitrile

274901-16-5

vildagliptin

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In tetrahydrofuran; butanone at 40℃; for 3h;82%
With potassium carbonate; potassium iodide In tetrahydrofuran; butanone at 40℃; for 3h; Reflux;82%
With potassium carbonate; potassium iodide In acetone at 50 - 55℃; for 3h; Solvent;82.2%
702-82-9

3-aminoadamantan-1-ol

(S)-pyrrolidine-2-carbonitrile p-toluenesulfonate

79-04-9

chloroacetyl chloride

274901-16-5

vildagliptin

Conditions
ConditionsYield
Stage #1: (S)-pyrrolidine-2-carbonitrile p-toluenesulfonate; chloroacetyl chloride With triethylamine In dichloromethane at 0 - 5℃; for 2h;
Stage #2: 3-aminoadamantan-1-ol In water for 4h; Temperature; Reflux;
76.9%

(S)-1-[2-(3-hydroxyadamantan-1-ylamino)acetyl]pyrrolidine-2-carboxylic acid amide

274901-16-5

vildagliptin

Conditions
ConditionsYield
Stage #1: (S)-1-[2-(3-hydroxyadamantan-1-ylamino)acetyl]pyrrolidine-2-carboxylic acid amide With trifluoroacetic acid; trifluoroacetic anhydride In 2-methyltetrahydrofuran Reflux;
Stage #2: With potassium carbonate In 2-methyltetrahydrofuran; water at 5 - 10℃; Reagent/catalyst;
75%
With trichlorophosphate In dichloromethane at 10℃; for 4h; Reagent/catalyst; Solvent; Temperature; Time; Reflux;4.53 g
702-82-9

3-aminoadamantan-1-ol

214398-99-9

(S)-1-(2-chloroacetyl) pyrrolidine-2-carboxamide

274901-16-5

vildagliptin

Conditions
ConditionsYield
Stage #1: (S)-1-(2-chloroacetyl) pyrrolidine-2-carboxamide With trifluoroacetic anhydride In tetrahydrofuran at 20℃; for 2h; Cooling with ice;
Stage #2: 3-aminoadamantan-1-ol With potassium carbonate; potassium iodide In tetrahydrofuran at 40℃; for 8.5h; Time; Reflux;
71%

(S)-1-{2-[benzyl(3-hydroxyadamantan-1-yl)amino]acetyl}pyrrolidine-2-carbonitrile

274901-16-5

vildagliptin

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol at 20℃;61.5%
With palladium 10% on activated carbon; hydrogen In methanol for 22h;
214398-99-9

(S)-1-(2-chloroacetyl) pyrrolidine-2-carboxamide

274901-16-5

vildagliptin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 7.82 g / trifluoroacetic anhydride / tetrahydrofuran / 1 h / 20 °C
2: K2CO3 / tetrahydrofuran / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C
2: potassium carbonate; potassium iodide / tetrahydrofuran / 5 h / 60 - 65 °C
View Scheme
Multi-step reaction with 2 steps
1.1: 1,3,5-trichloro-2,4,6-triazine / N,N-dimethyl-formamide / 4 h / 35 - 48 °C
2.1: potassium carbonate; potassium iodide / butanone / 40 °C
2.2: 3 h / 38 - 75 °C
View Scheme
Multi-step reaction with 2 steps
1.1: trichlorophosphate / -5 - 20 °C
2.1: potassium carbonate; potassium iodide / acetone / 0.25 h / 20 °C
2.2: 40 - 65 °C
View Scheme
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    WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

    Zhuo Zhou Wen Xi Import and Export Co., Ltd. is a company mainly engaged in the export of pharmaceutical raw materials. Its parent company is (Wen Xi Pharma), including three subs

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-13111626072

    Address:Room 1710, Baoxin International Phase I, 19 Guanyun East Road, Zhuozhou, Hebei

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  • BLOOM TECH Advanced API/Technology support Vildagliptin CAS 274901-16-5

  • Casno:

    274901-16-5

    MSDS/COA Download

    BLOOM TECH Advanced API/Technology support Vildagliptin CAS 274901-16-5

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

    Inquiry guide 1.Please send the quantity(Weight) to us, we will arrange our sales to provide the one-for-one service for you. 2.Then we will provide the professional quotation list for you, it will be including all the factors in who

    WHO WE ARE 1.We Focus on the technology of Organic Synthesis since 2008. 2.API/Pharmaceutical intermediate/Fine chemical/New material/Extraction etc. 3.Chemical reagent: Over 300,0

  •  Shaanxi BLOOM TECH Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-29-86470566

    Address:Block A of Central Mansion, No.113 of Weiyang Rd, ETDZ, Xi'an, Shaanxi 710016, China

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  • Vildagliptin CAS:274901-16-5 china supplier Free of customs clearance

  • Casno:

    274901-16-5

    Vildagliptin CAS:274901-16-5 china supplier Free of customs clearance

    Min.Order: 1 Kilogram

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    What's our company advantages 1. Government support guarantees good company credibility and finance safe. 2. Finer chem is confident at the quality of the products, and would like to supply free sample to our customers. 3. Factory locates in n

    Mulei (Wuhan) New Material Technology Co. Ltd is a scientific and technological company integrating product research and development, manufacture and trading of chemical intermedia

  •  WUHAN MULEI NEW MATERIAL CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8619831967063

    Address:Office1201#, Block C, Hanjie Headquarters International Plaza, Zhongbei Rd, Wuchang District, Wuhan

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  • Vildagliptin

  • Casno:

    274901-16-5

    Vildagliptin

    Min.Order: 1 Kilogram

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    High quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle

    Our company was established in May,2022, Changchun Weiersi Import and Export trade Co., Ltd, a professional manufacturer and exporter that is concerned with the design, development

  •  CHANGCHUN WEIERSI IMPORT AND EXPORT TRADE CO.,LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-431-80606858

    Address:547#West Min Zhu Street,Chaoyang District,Changchun City,Jilin Province,China

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  • High purity Vildagliptin CAS 274901-16-5 supplied by Chinese manufacturer

  • Casno:

    274901-16-5

    High purity Vildagliptin CAS 274901-16-5 supplied by Chinese manufacturer

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    1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appearance:Powder Storage:-20°C Freezer Package:1kg/foil bag; 1kg/tin ;

    Wuhan Fortuna Chemical Co., Ltd, located in the predominant Wu Han City where is a traffic hinge of China, is a big integrative chemical enterprise being engaged in producing and

  •  Wuhan Fortuna Chemical Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-27-59207850

    Address:A2705,Dong Yi Shi Qu,129# XinHua Road,WuHan,China

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  • Good Quality Vildagliptin CAS 274901-16-5 Glyptins for Antidiabetic

  • Casno:

    274901-16-5

    Good Quality Vildagliptin CAS 274901-16-5 Glyptins for Antidiabetic

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 200.0-400.0/Kilogram

    Hanways chempharm is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. The marketing department is located in Wuhan. We have two GMP facilities in Hubei Pr

    Hubei Hanways Pharmchem Co.,Limited is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. Now we

  •  HANWAYS CHEMPHARM CO.,LIMITED

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-18502787239(whatsapp)

    Address:18-1-802, Green Garden, Jianghan District, Wuhan 430023, China

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  • Vildagliptin,

  • Casno:

    274901-16-5

    Vildagliptin,

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

    Vildagliptin Chemical Properties Melting point 153-155 C alpha -78.3° (c = 9.73 in methanol) Boiling point 531.3±50.0 °C(Predicted) density 1.27 Fp 275.1℃ storage temp. Keep in dark place,Inert atmosphere,Store

    SHANGHAI MINSTAR CHEMICAL CO., LTD. is a leading, experienced, professional supplier of API & intermediates, plant extract, food additive, fine chemicals and industry chemicals, et

  •  Shanghai Minstar Chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-21-18019205509

    Address:BUILDING 8, NO.1098, CHUANSHA ROAD, SHANGHAI, CHINA

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  • 2-Pyrrolidinecarbonitrile,1-[2-[(3-hydroxytricyclo[3.3.1.13,7]dec-1-yl)amino]acetyl]-, (2S)-

  • Casno:

    274901-16-5

    2-Pyrrolidinecarbonitrile,1-[2-[(3-hydroxytricyclo[3.3.1.13,7]dec-1-yl)amino]acetyl]-, (2S)-

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

    The company is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds,

  •  Henan Wentao Chemical Product Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-370-2722992

    Address:32 Room, 5th Floor, Building 11, No. 6 Yinxing Road, High-tech Industrial Development Zone, Zhengzhou City, Henan Province

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  • 274901-16-5 CAS 99% BP USAP Vildagliptin

  • Casno:

    274901-16-5

    274901-16-5 CAS 99% BP USAP Vildagliptin

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0/Kilogram

    Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage:Refer to COA

    Our company was funded in 2018. In order to adapt to the trend of world development, we established B2B e-commerce sector in Hangzhou. We supply raw material of chemicals, like API

  •  Hangzhou Fonlynn Health Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86 13291832373

    Address:Room 622, Building 11, Yifeng City, Nanyuan Street, Yuhang District

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  • Vildagliptin Manufacturer/Cas:274901-16-5 / Viglistine99.8% High purity

  • Casno:

    274901-16-5

    Vildagliptin Manufacturer/Cas:274901-16-5 / Viglistine99.8% High purity

    Min.Order: 25 Metric Ton

    FOB Price:  USD $ 3.0-5.0/Metric Ton

    Chinese Name: Vildagliptin Chinese alias: Viglistine; Tardinalane; (-) - (2S) - 1 - [(3-hydroxy tricyclic [3.3.1.1 [3,7]] decane-1-amino] acetyl] pyrrolidine-2-methanonitrile; English Name: Vildagliptin English alias: Unii-I6B4B2U96p; Laf

    Hubei DiBo chemical co., LTD Hubei DiBo Chemical Co., Ltd. was founded in 2009, is located in Hubei Province on both sides of the Yangtze River, one of the ancient cities of Chines

  •  Hubei DiBo chemical co., LTD

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86 15871366807

    Address:No. 782 of wuchang district of wuhan city, hubei province

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  • Vildagliptin

  • Casno:

    274901-16-5

    Vildagliptin

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 1300.0-1400.0/Kilogram

    Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

    Baoji Guokang Healthchem co.,ltd located in Baoji High-tech Zone,is epitomizing international,cooperative and honest.We are a young company full of action and energy,and our profes

  •  Baoji Guokang Healthchem co.,ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-917-3909592

    Address:China

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  • Vildagliptin CAS: 274901-16-5

  • Casno:

    274901-16-5

    Vildagliptin CAS: 274901-16-5

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0/Gram

    Vildagliptin CAS: 274901-16-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia

    Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, speciali

  •  Qingdao Beluga Import and Export Co., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8613854236000

    Address:qingdao

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