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4637-24-5

Basic Information
CAS No.: 4637-24-5
Name: N,N-Dimethylformamide dimethyl acetal
Article Data: 37
Cas Database
Molecular Structure:
Molecular Structure of 4637-24-5 (N,N-Dimethylformamide dimethyl acetal)
Formula: C5H13NO2
Molecular Weight: 119.164
Synonyms: Trimethylamine,1,1-dimethoxy- (6CI,7CI,8CI);(Dimethoxymethyl)dimethylamine;(Dimethylamino)dimethoxymethane;(Dimethylamino)formaldehyde dimethyl acetal;1,1-Dimethoxy-N,N-dimethylmethanamine;1,1-Dimethoxy-N,N-dimethylmethane amine;1,1-Dimethoxytrimethylamine;DMF dimethyl acetal;DMFDMA;Dimethoxy(dimethylamino)methane;Dimethoxy-N,N-dimethylmethanamine;Dimethyl dimethylformamide acetal;Methyl-8;N,N-Dimethyl-1,1-bis(methyloxy)methanamine;N,N-Dimethylformamide dimethylacetal;N-(Dimethoxymethyl)-N,N-dimethylamine;N-(Dimethoxymethyl)dimethylamine;a,a-Dimethoxytrimethylamine;N,N-dimethylformamide dimethyl acetal (DMF-DMA);
EINECS: 225-063-3
Density: 0.906 g/cm3
Melting Point: -85 °C
Boiling Point: 104.3 °C at 760 mmHg
Flash Point: 7.2 °C
Solubility: hydrolysis with water
Appearance: clear colourless liquid
Hazard Symbols: FlammableF, HarmfulXn, IrritantXi
Risk Codes: 11-22-36/37/38-36/38-20-20/21/22-10
Safety: 16-26-36/37-36/37/39-33-29-7/9
Transport Information: UN 3271 3/PG 2
PSA: 21.70000
LogP: 0.12440
Synthetic route
124-41-4

sodium methylate

68-12-2, 33513-42-7

N,N-dimethyl-formamide

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-formamide With dimethyl sulfate at 20 - 70℃; for 4h;
Stage #2: sodium methylate at 25℃; for 2h; Temperature;
85.4%
124-40-3

dimethyl amine

149-73-5

trimethyl orthoformate

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
With acetyl chloride at 20℃; for 12h; Inert atmosphere;95%
1196967-42-6

C14H21NO3

1196967-61-9

C31H32N4O9S

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
With sulfuric acid In 1,4-dioxane; water at 0℃; for 6h; Inert atmosphere;80%
21511-55-7, 34643-89-5

(methoxymethylidene)dimethylammonium methyl sulfate

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
With methanol; sodium methylate at 0 - 20℃; for 20h; Inert atmosphere;59%
52117-32-5

chloro-dimethoxy-methane

124-40-3

dimethyl amine

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
at 140 - 150℃; for 2h; Green chemistry;86.8%
68-12-2, 33513-42-7

N,N-dimethyl-formamide

77-78-1

dimethyl sulfate

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
With nitrogen at 80℃; for 2h;100%
With sodium 1.) 3 h, 60-80 degC: 2.) 0 degC, methanol; Yield given. Multistep reaction;
at 60℃; for 3h;
124-41-4

sodium methylate

21511-55-7, 34643-89-5

(methoxymethylidene)dimethylammonium methyl sulfate

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
In Petroleum ether at 0℃; for 2h;
1192-62-7

1-(2-furyl)-1-ethanone

A

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

B

109482-86-2

(2E)-3-(dimethylamino)-1-furan-2-ylprop-2-en-1-one

350-03-8

methyl-3-pyridylketone

A

55314-16-4, 75415-01-9, 123367-26-0

(E)-3-(dimethylamino)-1-(pyridin-3-yl)prop-2-en-1-one

B

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

68-12-2, 33513-42-7

N,N-dimethyl-formamide

154147-42-9

2-butyl-2-imidazolin-5-one

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Conditions
ConditionsYield
With trichlorophosphate at 40℃; Condensation;
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Chemistry

The Molecular Structure of N,N-Dimethylformamide dimethyl acetal (CAS NO.4637-24-5):

Empirical Formula: C5H13NO2
Molecular Weight: 119.1622 
IUPAC Name: 1,1-dimethoxy-N,N-dimethylmethanamine 
Appearance: clear colourless liquid
Nominal Mass: 119 Da
Average Mass: 119.1622 Da
Monoisotopic Mass: 119.094629 Da 
Index of Refraction: 1.407
Molar Refractivity: 32.38 cm3
Molar Volume: 131.4 cm3
Surface Tension: 24.8 dyne/cm
Density: 0.906 g/cm3
Flash Point: 7.2 °C
Enthalpy of Vaporization: 34.33 kJ/mol
Boiling Point: 104.3 °C at 760 mmHg
Vapour Pressure: 31.1 mmHg at 25°C 
Storage temp: Fammables area
Water Solubility: hydrolysis
Sensitive: Moisture Sensitive
InChI
InChI=1/C5H13NO2/c1-6(2)5(7-3)8-4/h5H,1-4H3
Smiles
O(C(OC)N(C)C)C
Product Categories: blocks;BuildingBlocks;Aliphatics;(intermediate of zaleplon);Biochemistry;Nucleosides, Nucleotides & Related Reagents;Protecting Agents for Hydroxyl and Amino Groups;Protecting Agents, Phosphorylating Agents & Condensing Agents;Analytical Chemistry;Esterification & Alkylation (GC Derivatizing Reagents);GC Derivatizing Reagents;N,N-Dimethylformamide Dialkylacetals (GC Derivatizing Reagents)

Uses

 N,N-Dimethylformamide dimethyl acetal (CAS NO.4637-24-5) can be used as  intermediates of Zaleplon,also can be used as condensating agent.

Safety Profile

Hazard Codes: FlammableFIrritantXiIrritantXn
Risk Statements : 
R11: Highly Flammable 
R36/37/38: Irritating to eyes, respiratory system and skin
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed
R10: Flammable
Safety Statements : 
S16: Keep away from sources of ignition - No smoking 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S33: Take precautionary measures against static discharges 
S29: Do not empty into drains 
S7/9 :Keep container tightly closed and in a well-ventilated place
RIDADR: UN 3271 3/PG 2

Specification

 N,N-Dimethylformamide dimethyl acetal (CAS NO.4637-24-5) is also called as Dimethylformamide-dimethylacetal ; 1,1-Dimethoxytrimethylamine ; Methanamine, 1,1-dimethoxy-N,N-dimethyl- .