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5332-73-0

Basic Information
CAS No.: 5332-73-0
Name: 3-Methoxypropylamine
Article Data: 23
Cas Database
Molecular Structure:
Molecular Structure of 5332-73-0 (3-Methoxypropylamine)
Formula: C4H11NO
Molecular Weight: 89.1374
Synonyms: Propylamine,3-methoxy- (6CI,7CI,8CI);(3-Methoxypropan-1-yl)amine;1-Amino-3-methoxypropane;1-Methoxy-3-aminopropane;3-Amino-1-methoxypropane;3-Aminopropyl methyl ether;3-Methoxy-1-aminopropane;3-Methoxy-1-propanamine;3-Methoxy-n-propylamine;
EINECS: 226-241-3
Density: 0.852 g/cm3
Melting Point: -65 °C
Boiling Point: 118.3 °C at 760 mmHg
Flash Point: 22.8 °C
Solubility: Miscible with water
Appearance: clear, colorless liquid
Hazard Symbols: CorrosiveC
Risk Codes: 10-34-35
Safety: 26-36/37/39-45-16
Transport Information: UN 2734 8/PG 2
PSA: 35.25000
LogP: 0.68190
Synthetic route
105427-51-8

C6H5CHNCH2CH2CH2OCH3

5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
Stage #1: C6H5CHNCH2CH2CH2OCH3 With hydrogenchloride In cyclohexane at -10 - 0℃; for 14h;
Stage #2: With sodium carbonate In dichloromethane at -10 - 0℃; for 12h;
99.42%
110-67-8

3-Methoxypropionitrile

5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With hydrogen In methanol at 105 - 110℃; under 15001.5 - 22502.3 Torr; for 0.5h; Temperature; Pressure; Solvent; Autoclave;97.2%
With hydrogen at 60 - 98℃; under 1500.15 - 22502.3 Torr; for 6h; Temperature;95%
With hydrogenchloride; platinum(IV) oxide; hydrogen In ethanol under 2280 Torr; for 4h;30%
With ammonia; hydrogen; Rh catalyst under 51485.6 Torr;
110-67-8

3-Methoxypropionitrile

A

14676-58-5

bis-(3-methoxy-propyl)-amine

B

5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With ammonia; nickel at 90℃; Hydrogenation.unter Druck;
With nickel at 110℃; Hydrogenation.unter Druck;
22483-13-2

(3-Methoxy-propyl)-[2-methyl-prop-(Z)-ylidene]-amine

5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
In water at 35℃; Equilibrium constant;
41081-98-5

2-<(3-methoxy)propyl>-isoindole-1,3(2H)-dione

5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With hydrazine
77-78-1

dimethyl sulfate

156-87-6

propan-1-ol-3-amine

A

20650-07-1

3-(Dimethylamino)-1-propyl Methyl Ether

B

55612-03-8

N-[3-(methoxy)propyl]-N-methylamine

C

5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With calcium hydride 1.) THF, room temp., 1 h; 2.) room temp., 1 h; Yield given. Multistep reaction;
With sodium hydride 1.) THF, room temp., 1 h; 2.) room temp., 1 h; Yield given. Multistep reaction;
24424-99-5

di-tert-butyl dicarbonate

5332-73-0

3-methoxypropylamine

911300-60-2

tert-butyl (3-methoxypropyl)carbamate

Conditions
ConditionsYield
In chloroform for 16h; Heating / reflux;100%
165450-61-3

2-hydroxy-3-(1-methyl-1-phenylethyl)benzaldehyde

5332-73-0

3-methoxypropylamine

1096704-38-9

C20H25NO2

Conditions
ConditionsYield
In ethanol at 20℃; for 6h;100%
98-03-3

thiophene-2-carbaldehyde

5332-73-0

3-methoxypropylamine

1227253-60-2

3-methoxy-N-(thiophen-2-ylmethylene)propanamine

Conditions
ConditionsYield
at 60℃; for 6h; Inert atmosphere;100%
87-42-3

6-chloro-3H-purine

5332-73-0

3-methoxypropylamine

(3-methoxypropyl)(3H-purin-6-yl)amine

Conditions
ConditionsYield
In butan-1-ol at 100℃; for 16h;100%
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Consensus Reports

Reported in EPA TSCA Inventory.

Specification

3-Methoxypropylamine, with CAS number of 5332-73-0, can be called Propylamine,3-methoxy- (6CI,7CI,8CI); (3-Methoxypropan-1-yl)amine; 1-Amino-3-methoxypropane; 1-Methoxy-3-aminopropane; 3-Amino-1-methoxypropane; 3-Aminopropyl methyl ether; 3-Methoxy-n-propylamine. It is a clear colourless to faintly colored liquid. 3-Methoxypropylamine is used as intermediate in the production of: dyestuff, corrosion inhibitor.

Physical properties about 3-Methoxypropylamine are: (1)ACD/LogP: -0.44; (2)ACD/LogD (pH 5.5): -3.51; (3)ACD/LogD (pH 7.4): -2.70; (4)ACD/BCF (pH 5.5): 1.00; (5)ACD/BCF (pH 7.4): 1.00; (6)ACD/KOC (pH 5.5): 1.00; (7)ACD/KOC (pH 7.4): 1.00; (8)#H bond acceptors: 2; (9)#H bond donors: 2; (10)#Freely Rotating Bonds: 4; (11)Index of Refraction: 1.409; (12)Molar Refractivity: 25.861 cm3; (13)Molar Volume: 104.602 cm3; (14)Polarizability: 10.252 10-24cm3; (15)Surface Tension: 27.7099990844727 dyne/cm; (16)Density: 0.852 g/cm3; (17)Flash Point: 22.778 °C; (18)Enthalpy of Vaporization: 35.655 kJ/mol; (19)Boiling Point: 118.317 °C at 760 mmHg; (20)Vapour Pressure: 16.7590007781982 mmHg at 25°C

When you are using this chemical, please be cautious about it as the following:
1. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice;
2. Wear suitable protective clothing, gloves and eye/face protection;
3. In case of accident or if you feel unwell, seek medical advice immediately (show label where possible);
4. Keep away from sources of ignition - No smoking;

You can still convert the following datas into molecular structure:
(1)InChI=1S/C4H11NO/c1-6-4-2-3-5/h2-5H2,1H3;
(2)InChIKey=FAXDZWQIWUSWJH-UHFFFAOYSA-N;
(3)SmilesC(COC)CN

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intravenous 180mg/kg (180mg/kg)   U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#03063,