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625-36-5

Basic Information
CAS No.: 625-36-5
Name: Propanoylchloride, 3-chloro-
Molecular Structure:
Molecular Structure of 625-36-5 (Propanoylchloride, 3-chloro-)
Formula: C3H4Cl2O
Molecular Weight: 126.97
Synonyms: Propionylchloride, 3-chloro- (6CI,7CI,8CI);(Chloromethyl)acetyl chloride;3-Chloropropanoyl chloride;3-Chloropropionic acid chloride;NSC 84180;b-Chloropropanoylchloride;b-Chloropropionic acid chloride;b-Chloropropionyl chloride;w-Chloropropanoyl chloride;w-Chloropropionyl chloride;
EINECS: 210-890-4
Density: 1.296 g/cm3
Melting Point: -32 °C
Boiling Point: 144.9 °C at 760 mmHg
Flash Point: 61.7 °C
Solubility: reacts with water
Appearance: Clear colorless to dark brown liquid
Hazard Symbols: VeryT+
Risk Codes: 14-22-26-34-35-10
Safety: 23-26-36/37/39-45-38-16-8
Transport Information: UN 3390 6.1/PG 1
PSA: 17.07000
LogP: 1.38070
Synthetic route
107-94-8

chloropropionic acid

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With bis(trichloromethyl) carbonate In toluene at 25℃; for 8h; Reagent/catalyst; Temperature;98.5%
With thionyl chloride63%
With phosphorus trichloride
57-57-8

β-Propiolactone

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With bis(trichloromethyl) carbonate; N,N-dimethylpiperidine-4-carboxamide hydrochloride at 25℃; for 10h; Reagent/catalyst; Large scale;98%
With phosphorus pentachloride In benzene at 20℃; for 10h; Chlorination;87%
With tetrachloromethane; sulfuryl dichloride
With tetrachloromethane; phosphorus pentachloride
With thionyl chloride
79-10-7

acrylic acid

A

814-68-6

acryloyl chloride

B

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With thionyl chloride In N,N-dimethyl-formamide at 80℃; under 2068.65 Torr; for 0.416667h; Reagent/catalyst; Pressure;A 4%
B 94%
With trichlorophosphate In N,N-dimethyl-formamide at 80℃; for 0.00833333h; Reagent/catalyst; Temperature;A 91%
B 6%
With thionyl chloride; N,N-dimethyl-formamide In neat (no solvent) at 60℃; for 0.0166667h; Catalytic behavior; Reagent/catalyst; Temperature; Time; Flow reactor;
79-10-7

acrylic acid

A

C6H7ClO3

B

814-68-6

acryloyl chloride

C

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With thionyl chloride In N,N-dimethyl-formamide at 60℃; for 0.0166667h; Reagent/catalyst;A 7%
B 82%
C 11%
79-10-7

acrylic acid

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With phosgene; N,N-dimethyl-formamide at 70℃; for 10h;80%
With N,N-dimethyl-formamide
With phosgene In N,N-dimethyl-formamide at 70℃; for 40h;
With phosgene In N,N-dimethyl-formamide at 70℃; for 40h;200 g
With thionyl chloride In N,N-dimethyl-formamide at 80℃; for 0.416667h; Concentration; Reagent/catalyst;
676-83-5

methyldichlorophosphane

79-10-7

acrylic acid

A

15171-48-9

2-methyl-2,5-dioxo-1,2-oxaphospholane

B

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
In paraffinA n/a
B 76%
A n/a
B 76%
23270-34-0

3-(chloro-methyl-phosphinoyl)-butyryl chloride

79-10-7

acrylic acid

A

2,4-Dimethyl-2,5-dioxo-1,2-phospholane

2,4-Dimethyl-2,5-dioxo-1,2-phospholane

B

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
A n/a
B 70%
15171-48-9

2-methyl-2,5-dioxo-1,2-oxaphospholane

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
70%
75-44-5

phosgene

74-85-1

ethene

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With aluminium trichloride; toluene
With carbon disulfide at -5 - -4℃;
79-03-8

propionyl chloride

A

7623-09-8

2-chloropropionyl chloride

B

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With chlorine at 0 - 5℃; Irradiation.unter UV-Bestrahlung;
With sulfuryl dichloride; dibenzoyl peroxide
With sulfuryl dichloride; dibenzoyl peroxide
79-03-8

propionyl chloride

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
With chlorine at 0 - 5℃; Irradiation.UV-Bestrahlung;
With sulfuryl dichloride; dibenzoyl peroxide
74-85-1

ethene

201230-82-2

carbon monoxide

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
(i) PdCl2, benzene, (ii) /BRN= 3587209/; Multistep reaction;
107-13-1

acrylonitrile

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
(i) aq. HCl, (ii) SOCl2; Multistep reaction;
7719-09-7

thionyl chloride

57-57-8

β-Propiolactone

625-36-5

2-chloropropionyl chloride

57-57-8

β-Propiolactone

10026-13-8, 874483-75-7

phosphorus pentachloride

625-36-5

2-chloropropionyl chloride

56-23-5

tetrachloromethane

79-03-8

propionyl chloride

A

625-36-5

2-chloropropionyl chloride

B

α-chloro-propionyl chloride

α-chloro-propionyl chloride

Conditions
ConditionsYield
Chlorierung unter Belichtung;
79-03-8

propionyl chloride

7782-50-5

chlorine

A

7623-09-8

2-chloropropionyl chloride

B

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
at 0 - 5℃; UV-Bestrahlung.Irradiation;
7791-25-5

sulfuryl dichloride

79-03-8

propionyl chloride

94-36-0

dibenzoyl peroxide

A

7623-09-8

2-chloropropionyl chloride

B

625-36-5

2-chloropropionyl chloride

79-03-8

propionyl chloride

A

625-36-5

2-chloropropionyl chloride

B

α-chloro-propionic acid chloride

α-chloro-propionic acid chloride

Conditions
ConditionsYield
With tetrachloromethane; chlorine
75-44-5

phosgene

7446-70-0

aluminium trichloride

74-85-1

ethene

108-88-3

toluene

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
at 35 - 40℃;
75-44-5

phosgene

7446-70-0

aluminium trichloride

74-85-1

ethene

CS2

CS2

625-36-5

2-chloropropionyl chloride

Conditions
ConditionsYield
at -7 - -2℃;
635-46-1

1,2,3,4-tetrahydroisoquinoline

625-36-5

2-chloropropionyl chloride

57369-31-0

1,2,6,7-tetrahydropyrido<3,2,1-i,j>quinolin-3(5H)-one

Conditions
ConditionsYield
Stage #1: 1,2,3,4-tetrahydroisoquinoline; 2-chloropropionyl chloride In acetone for 1h; Inert atmosphere; Reflux;
Stage #2: With aluminum (III) chloride; sodium chloride at 150℃; for 1h; Inert atmosphere;
100%
Stage #1: 1,2,3,4-tetrahydroisoquinoline; 2-chloropropionyl chloride In acetone for 1h; Reflux;
Stage #2: With aluminum (III) chloride; sodium chloride at 150℃; for 0.5h;
88%
With acetone Erhitzen des Reaktionsprodukts mit Aluminiumchlorid;
With aluminium trichloride 1.) acetone, reflux, 2 h, 2.) heating; Multistep reaction;
106-49-0

p-toluidine

625-36-5

2-chloropropionyl chloride

19342-88-2

3-chloro-N-(4-methylphenyl)propionamide

Conditions
ConditionsYield
In acetone for 1h; Acylation; Heating;100%
In water; acetone for 6h; Reflux;100%
With potassium carbonate In acetone at 0℃; for 1h; Condensation;95%
106-47-8

4-chloro-aniline

625-36-5

2-chloropropionyl chloride

19314-16-0

3-chloro-N-(4-chlorophenyl)propanamide

Conditions
ConditionsYield
In acetone for 1h; Acylation; Heating;100%
In acetone for 2h; Reflux;85%
Stage #1: 4-chloro-aniline With sodium acetate; acetic acid In water at 5℃;
Stage #2: 2-chloropropionyl chloride at 0 - 20℃;
70%
64-04-0

phenethylamine

625-36-5

2-chloropropionyl chloride

306-20-7

3-chloro-N-(4-phenylethyl)propanamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In chloroform; water at 20℃; for 1h;100%
With sodium hydroxide
100-01-6

4-nitro-aniline

625-36-5

2-chloropropionyl chloride

19313-88-3

3-chloro-N-(4-nitrophenyl)propanamide

Conditions
ConditionsYield
at 0 - 50℃; Neat (no solvent);100%
at 20 - 50℃;100%
at 50℃; for 16h;97%
62-53-3

aniline

625-36-5

2-chloropropionyl chloride

3460-04-6

3-chloro-N-phenylpropionamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 2h;100%
With potassium carbonate In acetone at 0℃; for 1h; Condensation;98%
With potassium carbonate In water; acetone at 0℃; for 1h;98%
91-20-3

naphthalene

625-36-5

2-chloropropionyl chloride

22422-70-4

3-chloro-1-(naphthalen-2-yl)propan-1-one

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 20℃; Cooling with ice;100%
With carbon disulfide; aluminium trichloride
With aluminium trichloride In nitrobenzene 1.) 5 h, room temp., 2.) 30 min, 40-45 deg C;
Stage #1: naphthalene; 2-chloropropionyl chloride With aluminum (III) chloride In nitrobenzene at 0℃;
Stage #2: With hydrogenchloride In nitrobenzene
4235-20-5

5-chloro-2-phenylsulfanyl-aniline

625-36-5

2-chloropropionyl chloride

101096-34-8

N-(3-chloropropyl)-5-chloro-2-phenylthiophenylamine

Conditions
ConditionsYield
With pyridine In diethyl ether at 0℃; for 0.333333h;100%
625-36-5

2-chloropropionyl chloride

71-43-2

benzene

936-59-4

3-chloropropiophenone

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Inert atmosphere;100%
aluminium trichloride; nitromethane In carbon disulfide for 2h; Product distribution; Mechanism; Ambient temperature; further Friedel-Crafts catalysts, further arenes, further haloacid chlorides; variation of temperature and time;88%
aluminium trichloride; nitromethane In carbon disulfide for 2h; Ambient temperature;88%
188290-36-0

thiophene

625-36-5

2-chloropropionyl chloride

40570-64-7

3-chloro-1-(2-thienyl)propan-1-one

Conditions
ConditionsYield
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at -5℃; for 0.166667h; Friedel Crafts Acylation;
Stage #2: thiophene In dichloromethane at -5℃; for 1h; Friedel Crafts Acylation;
100%
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at 20℃; for 0.25h;
Stage #2: thiophene In dichloromethane at 0 - 20℃; for 4h;
99%
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at 20℃; for 0.25h;
Stage #2: thiophene In dichloromethane at 0 - 20℃; for 4h;
99%
496-15-1

1-indoline

625-36-5

2-chloropropionyl chloride

64140-62-1

N-(β-chloropropionyl)-indoline

Conditions
ConditionsYield
In acetone at 70℃; for 3h;100%
In acetone at 70℃; for 3h; Inert atmosphere; Sealed tube;99%
In acetone for 1h; Reflux;73%
136304-78-4

methyl 3-amino-2-[[(2'-cyanobiphenyl-4-yl)methyl]amino]benzoate

625-36-5

2-chloropropionyl chloride

136304-79-5

methyl 2-(2-chloroethyl)-1-[(2'-cyanobiphenyl-4-yl)methyl]benzimidazole-7-carboxylate

Conditions
ConditionsYield
In dichloromethane for 2h; Ambient temperature;100%
With hydrogenchloride In methanol; CH2 Cl2 -H2 O; dichloromethane
625-36-5

2-chloropropionyl chloride

102-56-7

2,5-dimethoxyaniline

N-(2',5'-dimethoxyphenyl)-3-chloropropanamide

Conditions
ConditionsYield
In benzene for 1h; Ambient temperature;100%
50399-51-4, 215371-20-3

trans-1,2,3,4-tetrahydro-7-methoxy-1-naphthylamine

625-36-5

2-chloropropionyl chloride

N-(7-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)-3-chloropropanamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane100%
625-36-5

2-chloropropionyl chloride

2039-67-0

2-(3-methoxyphenyl)-1-ethanamine

34164-26-6

3-chloro-N-[2-(3-methoxyphenyl)ethyl]propionamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In chloroform; water at 20℃; for 1h;100%
21835-63-2

1,4-dihydro-4-(3-aminophenyl)-2,6-dimethyl-3,5-pyridinedicarboxylic acid,dimethyl ester

625-36-5

2-chloropropionyl chloride

1,4-Dihydro-4-[3-[[3-chloro-1-oxo-1-propyl]amino]phenyl]-2,6-dimethyl-3,5-pyridinedicarboxylic acid, dimethyl ester

Conditions
ConditionsYield
In tetrahydrofuran; ethyl acetate100%
In tetrahydrofuran; ethyl acetate100%
In tetrahydrofuran; ethyl acetate100%
19727-83-4

6-nitroindoline

625-36-5

2-chloropropionyl chloride

1-(3-Chloropropionyl)6-nitroindoline

Conditions
ConditionsYield
With hydrogenchloride In acetone100%
625-36-5

2-chloropropionyl chloride

98384-97-5

C3H4ClN3O

Conditions
ConditionsYield
With sodium azide100%
848139-78-6

6-amino-4-((3-chloro-4-(pyridin-2-ylmethoxy)phenyl)amino)-7-ethoxyquinoline-3-carbonitrile

625-36-5

2-chloropropionyl chloride

1233953-82-6

3-chloro-N-(4-(3-chloro-4-(pyridin-2-ylmethoxy)anilino)-3-cyano-7-ethoxyquinolin-6-yl)propanamide

Conditions
ConditionsYield
at 50℃; for 16h;100%
at 50℃;99%
1750-42-1

3-aminoisoxazole

625-36-5

2-chloropropionyl chloride

1225869-37-3

3-chloro-N-(isoxazol-3-yl)propanamide

Conditions
ConditionsYield
Stage #1: 3-aminoisoxazole With sodium hydride In tetrahydrofuran; mineral oil for 6h; Inert atmosphere;
Stage #2: 2-chloropropionyl chloride In tetrahydrofuran; mineral oil at 20℃; Inert atmosphere;
100%

N1-(2-(dimethylamino)ethyl)-5-methoxy-N4-(2-((2-methoxy-4-(3-(methylsulfonyl)propoxy)phenyl)amino)-5-(trifluoromethyl)pyrimidin-4-yl)-N1-methylbenzene-1,2,4-triamine

625-36-5

2-chloropropionyl chloride

3-chloro-N-(2-((2-(dimethylamino)ethyl)(methyl)amino)-4-methoxy-5-((2-((2-methoxy-4-(3-(methylsulfonyl)propoxy)phenyl)amino)-5-(trifluoromethyl)pyrimidin-4-yl)amino)phenyl)propanamide

Conditions
ConditionsYield
In tetrahydrofuran; water at 25℃; for 2h;100%
27407-11-0

3-bromo-4-fluorophenol

625-36-5

2-chloropropionyl chloride

3-bromo-4-fluorophenyl 3-chloropropanoate

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at -50 - 20℃;100%
With aluminum (III) chloride In dichloromethane at -50 - 20℃;71%

11-aminosampangine

625-36-5

2-chloropropionyl chloride

C18H12ClN3O2

Conditions
ConditionsYield
Reflux;100%
6638-79-5

N,O-dimethylhydroxylamine*hydrochloride

625-36-5

2-chloropropionyl chloride

1062512-53-1

3-chloro-N-methoxy-N-methylpropanamide

Conditions
ConditionsYield
With potassium carbonate In diethyl ether; water at 0 - 20℃; Inert atmosphere;99.9%
With potassium carbonate In diethyl ether; water at 0 - 20℃; Inert atmosphere;92%
With potassium carbonate In tetrahydrofuran; water at 0 - 20℃; Inert atmosphere;
75-64-9

tert-butylamine

625-36-5

2-chloropropionyl chloride

100859-81-2

N-tert-butyl-2-(chloromethyl)acetamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane; water at -20 - 20℃; for 2h;99%
With sodium hydroxide; 1,2-dichloro-ethane
95-47-6

o-xylene

625-36-5

2-chloropropionyl chloride

22422-23-7

3-chloro-1-(3,4-dimethyl-phenyl)-propan-1-one

Conditions
ConditionsYield
With aluminum (III) chloride; nitromethane at 19 - 22℃; under 760.051 Torr; Friedel Crafts acylation; Inert atmosphere;99%
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts acylation; Inert atmosphere;98%
With aluminum (III) chloride In dichloromethane at 25℃; for 3h;96%
100-74-3

N-ethylmorpholine;

625-36-5

2-chloropropionyl chloride

N-ethyl-N-(3-propanoyl-N-ethylmorpholinium chloride) morpholinium chloride

Conditions
ConditionsYield
In benzene for 1h; Heating;99%
1077-16-3

hexylbenzene

625-36-5

2-chloropropionyl chloride

3-chloro-1-(4-hexylphenyl)-1-propanone

Conditions
ConditionsYield
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane at 20℃; for 0.25h;
Stage #2: hexylbenzene In dichloromethane at 20℃; for 24h;
99%
With aluminium trichloride In pentane at 20℃; for 1h;67%
553-94-6

4-bromo-m-xylene

625-36-5

2-chloropropionyl chloride

246022-83-3

4-bromo-1-(3'-chloro-1'-oxopropyl)-2,5-dimethylbenzene

Conditions
ConditionsYield
Stage #1: 2-chloropropionyl chloride With aluminum (III) chloride In dichloromethane for 0.25h; Schlenk technique; Inert atmosphere;
Stage #2: 4-bromo-m-xylene In dichloromethane at 20℃; for 20h; Inert atmosphere;
99%
With aluminium trichloride In dichloromethane at 50℃; for 3h; Addition;87%
With aluminum (III) chloride In carbon disulfide at 0℃; for 1h; Reflux;61%
With aluminium trichloride In carbon disulfide at 20℃; for 16h;
583-70-0

1-bromo-2,4-dimethylbenzene

625-36-5

2-chloropropionyl chloride

84092-78-4

1-(5-bromo-2,4-dimethylphenyl)-3-chloropropan-1-one

Conditions
ConditionsYield
With aluminium trichloride In carbon disulfide for 0.5h; Friedel-Crafts reaction; Heating;99%
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    3-Chloropropionyl chloride CAS: 625-36-5

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    Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an

    Located in Hangzhou National Hi-Tech Industrial Development Zone, Hangzhou zhongqi chem co.,Ltd is an ISO 9001:2015 & SGS certified molden chemical company,who is mainly focus on t

  •  Hangzhou Zhongqi chem Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:0086-571-86976032

    Address:Kangkang Gu 1010, Chun xiao road 61,Binjiang District 310052,Hangzhou city , China

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Chemistry

Molecular Structure of Propanoylchloride, 3-chloro- (CAS No.625-36-5):
 
Molecular Formula: C3H4Cl2O   
Molecular Weight: 126.9693
IUPAC Name: 3-Chloropropanoyl chloride 
CAS No: 625-36-5
H bond acceptors: 1
H bond donors: 0
Freely Rotating Bonds: 2
Polar Surface Area: 17.07 Å2
Index of Refraction: 1.437
Molar Refractivity: 25.67 cm3
Molar Volume: 97.9 cm3
Surface Tension: 32.2 dyne/cm
Density: 1.296 g/cm3
Flash Point: 61.7 °C
Enthalpy of Vaporization: 38.2 kJ/mol
Boiling Point: 144.9 °C at 760 mmHg
Vapour Pressure: 4.97 mmHg at 25°C
InChI: InChI=1/C3H4Cl2O /c4-2-1-3(5)6/h1-2H2
InChIKey: INUNLMUAPJVRME-UHFFFAOYAG
Std. InChI: InChI=1S/C3H4Cl2O /c4-2-1-3(5)6/h1-2H2
Std. InChIKey: INUNLMUAPJVRME-UHFFFAOYSA-N
Synonyms of Propanoylchloride, 3-chloro- (CAS No.625-36-5): .Beta.-Chloropropanoyl chloride ; .Beta.-Chloropropionoyl chloride ; .Beta.-Chloropropionyl chloride ; 3-Chloropropanoyl chloride ; 3-Chlorpropanoylchlorid ; Beta-Chloropropanoyl chloride ; Beta-Chloropropionoyl chloride ; Beta-Chloropropionyl chloride ; Chlorure de 3-chloropropanoyle ; Propanoyl chloride, 3-chloro-  
Product Categories: Halogen compounds;Acid Halides;Carbonyl Compounds;Organic Building Blocks

Safety Profile

Hazard Codes:VeryT+
Risk Statements:14-22-26-34-35-10
R14:Reacts violently with water. 
R22:Harmful if swallowed. 
R26:Very toxic by inhalation. 
R34:Causes burns. 
R35:Causes severe burns. 
R10:Flammable.
Safety Statements:23-26-36/37/39-45-38-16-8
S23:Do not breathe vapour. 
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection. 
S45:In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) 
S38:In case of insufficient ventilation, wear suitable respiratory equipment. 
S16:Keep away from sources of ignition. 
S8:Keep container dry.
RIDADR:UN 3390 6.1/PG 1
WGK Germany:1
F:21
HazardClass:6.1
PackingGroup:I
HS Code:29159080