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CAS No.: | 7148-50-7 |
---|---|
Name: | 5-Methyl-5-propyl-1,3-dioxan-2-one |
Article Data: | 8 |
Molecular Structure: | |
Formula: | C8H14O3 |
Molecular Weight: | 158.197 |
Synonyms: | 5-methyl-5-propyl-1,3-dioxan-2-one; |
Density: | 1.004g/cm3 |
Boiling Point: | 262.6°Cat760mmHg |
Flash Point: | 114.9°C |
PSA: | 35.53000 |
LogP: | 1.95960 |
phosgene
2-methyl-2-propyl-1,3-propanediol
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With antipyrine; chloroform |
2-methyl-2-propyl-1,3-propanediol
Diethyl carbonate
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With sodium methylate Entfernen des entstehenden Aethanols; | |
With sodium 1.) toluene, 90 deg C, 30 min, 2.) toluene, 88-110 deg C; Yield given. Multistep reaction; |
2-methyl-2-propyl-1,3-propanediol
bis(trichloromethyl) carbonate
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at -78 - 20℃; for 16h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: p-toluenesulfonyl chloride; n-butyllithium 1.2: 0 - 60 °C 2.1: C49H74AlNO4; bis(triphenylphosphoranylidene)ammonium iodide / butanone / 24 h / 110 °C / 7500.75 Torr / Autoclave; Sealed tube View Scheme |
3-methyl 3-n-propyl oxetane
carbon dioxide
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With C49H74AlNO4; bis(triphenylphosphoranylidene)ammonium iodide In butanone at 110℃; under 7500.75 Torr; for 24h; Autoclave; Sealed tube; |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
A
methanol
B
2-methyl-2-propyl-1,3-propanediol
Conditions | Yield |
---|---|
With [Mn(HN(C2H4PiPr2)2)(CO)2Br]; hydrogen; sodium t-butanolate In tetrahydrofuran at 120℃; under 22502.3 Torr; for 26h; Schlenk technique; Glovebox; Autoclave; | A 94% B 98% |
Conditions | Yield |
---|---|
With ammonia |
morpholine
5-Methyl-5-n-propyl-1,3-dioxan-2-one
morpholine-4-carboxylic acid 2-hydroxymethyl-2-methyl-pentyl ester
methamphetamin
5-Methyl-5-n-propyl-1,3-dioxan-2-one
2-Methyl-2-propyl-3--propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
1-amino-3-methylbutane
2-Methyl-2-propyl-3-<(3-methyl-butyl)-carbamoyl-oxy>-propanol-(1)