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7148-50-7

Basic Information
CAS No.: 7148-50-7
Name: 5-Methyl-5-propyl-1,3-dioxan-2-one
Article Data: 8
Molecular Structure:
Molecular Structure of 7148-50-7 (5-Methyl-5-propyl-1,3-dioxan-2-one)
Formula: C8H14O3
Molecular Weight: 158.197
Synonyms: 5-methyl-5-propyl-1,3-dioxan-2-one;
Density: 1.004g/cm3
Boiling Point: 262.6°Cat760mmHg
Flash Point: 114.9°C
PSA: 35.53000
LogP: 1.95960
Synthetic route
75-44-5

phosgene

78-26-2

2-methyl-2-propyl-1,3-propanediol

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

Conditions
ConditionsYield
With antipyrine; chloroform
78-26-2

2-methyl-2-propyl-1,3-propanediol

105-58-8

Diethyl carbonate

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

Conditions
ConditionsYield
With sodium methylate Entfernen des entstehenden Aethanols;
With sodium 1.) toluene, 90 deg C, 30 min, 2.) toluene, 88-110 deg C; Yield given. Multistep reaction;
78-26-2

2-methyl-2-propyl-1,3-propanediol

32315-10-9

bis(trichloromethyl) carbonate

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at -78 - 20℃; for 16h;
78-26-2

2-methyl-2-propyl-1,3-propanediol

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: p-toluenesulfonyl chloride; n-butyllithium
1.2: 0 - 60 °C
2.1: C49H74AlNO4; bis(triphenylphosphoranylidene)ammonium iodide / butanone / 24 h / 110 °C / 7500.75 Torr / Autoclave; Sealed tube
View Scheme
13911-97-2

3-methyl 3-n-propyl oxetane

124-38-9

carbon dioxide

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

Conditions
ConditionsYield
With C49H74AlNO4; bis(triphenylphosphoranylidene)ammonium iodide In butanone at 110℃; under 7500.75 Torr; for 24h; Autoclave; Sealed tube;
7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

A

67-56-1

methanol

B

78-26-2

2-methyl-2-propyl-1,3-propanediol

Conditions
ConditionsYield
With [Mn(HN(C2H4PiPr2)2)(CO)2Br]; hydrogen; sodium t-butanolate In tetrahydrofuran at 120℃; under 22502.3 Torr; for 26h; Schlenk technique; Glovebox; Autoclave;A 94%
B 98%
7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

1471-56-3

2-methyl-2-propyl-3-hydroxypropylcarbamate

Conditions
ConditionsYield
With ammonia
110-91-8

morpholine

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

25384-42-3

morpholine-4-carboxylic acid 2-hydroxymethyl-2-methyl-pentyl ester

7632-10-2

methamphetamin

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

25384-40-1

2-Methyl-2-propyl-3--propanol-(1)

7148-50-7

5-Methyl-5-n-propyl-1,3-dioxan-2-one

107-85-7

1-amino-3-methylbutane

25384-37-6

2-Methyl-2-propyl-3-<(3-methyl-butyl)-carbamoyl-oxy>-propanol-(1)

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