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75-16-1

Basic Information
CAS No.: 75-16-1
Name: Magnesium, bromomethyl-
Molecular Structure:
Molecular Structure of 75-16-1 (Magnesium, bromomethyl-)
Formula: CH3BrMg
Molecular Weight: 119.26
Synonyms: Methylmagnesiumbromide (6CI);Bromomethylmagnesium;
EINECS: 200-844-1
Density: 1.035 g/mL at 25 °C
Melting Point: 0oC
Boiling Point: 78-80 oC
Flash Point: -20 oC
Solubility: vigorous reaction with water
Appearance: Clear brown solution when properly stored
Hazard Symbols: FlammableF,CorrosiveC
Risk Codes: 12-14-19-22-34-66-67-52/53-10-65-63-48/20-14/15-11
Safety: 9-16-26-45-61-36/37/39-62-43-36/37-23
Transport Information: UN 3399 4.3/PG 1
PSA: 0.00000
LogP: 1.42940
Synthetic route
74-95-3

1,2-dibromomethane

A

187737-37-7

propene

B

74-85-1

ethene

C

75-16-1

methylmagnesium bromide

D

27329-47-1

methylenedimagnesium dibromide

E

MgBr2

MgBr2

Conditions
ConditionsYield
With amalgamated magnesium In diethyl ether; benzene at 0℃; special sealed glass apparatus; Further byproducts given;A n/a
B n/a
C n/a
D 50%
E n/a
74-83-9

methyl bromide

75-16-1

methylmagnesium bromide

Conditions
ConditionsYield
With magnesium In diethyl ether Thermodynamic data; -ΔH(reaction);
With magnesium at -258.2℃; Product distribution; codeposition with other metals under matrix isolation conditions;
With magnesium In diethyl ether
1493-13-6

trifluorormethanesulfonic acid

E-β-(dibenzylchlorosilyl)styrene

A

75-16-1

methylmagnesium bromide

B

C15H14ClF3O3SSi

Conditions
ConditionsYield
In dichloromethane
1493-13-6

trifluorormethanesulfonic acid

E-β-(benzyldiphenylsilyl)styrene

A

75-16-1

methylmagnesium bromide

B

C20H17F3O3SSi

Conditions
ConditionsYield
In dichloromethane
74-83-9

methyl bromide

magnesium

magnesium

75-16-1

methylmagnesium bromide

Conditions
ConditionsYield
With diethyl ether
87-41-2

2-benzofuran-1(3H)-one

75-16-1

methylmagnesium bromide

55549-01-4

α,α-dimethyl-o-xylene α,α'-diol

Conditions
ConditionsYield
at -78 - 20℃;100%
In tetrahydrofuran; diethyl ether at 30℃; for 12.5h;88%
unter Wasserabgabe entsteht 1.1-Dimethyl-phthalan;
75-16-1

methylmagnesium bromide

15174-47-7

α-methyl-trans-cinnamaldehyde

87422-10-4

(E)-3-methyl-4-phenyl-but-3-en-2-ol

Conditions
ConditionsYield
Stage #1: methylmagnesium bromide; α-methyl-trans-cinnamaldehyde In tetrahydrofuran; diethyl ether at 0℃; for 0.5h; Inert atmosphere;
Stage #2: With water; ammonium chloride In tetrahydrofuran; diethyl ether
100%
With diethyl ether
51934-41-9

4-iodobenzoic acid ethyl ester

75-16-1

methylmagnesium bromide

60514-82-1

2-(4-iodophenyl)propan-2-ol

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 72h;100%
22725-38-8

3-methoxy-5H-dibenzo[a,d]cyclohepten-5-one

75-16-1

methylmagnesium bromide

125025-18-5

3-methoxy-5-methyl-5H-dibenzocyclohepten-5-ol

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 6h; Ambient temperature;100%
112-45-8

10-Undecenal

75-16-1

methylmagnesium bromide

21951-49-5

dodec-11-en-2-ol

Conditions
ConditionsYield
In diethyl ether at -40℃; Grignard reaction;100%
In tetrahydrofuran at 0℃; Grignard reaction;90%
In tetrahydrofuran; diethyl ether at -40 - 25℃; for 15h; Inert atmosphere;83%
75-16-1

methylmagnesium bromide

82495-72-5

(E)-5-(N-benzyl-p-toluenesulfonamido)-3-methyl-6-phenylhex-3-on-2-one

82536-02-5

(E)-5-(N-benzyl-p-toluenefulfonamido)-2,3-dimethyl-6-phenylhex-3-en-2-ol

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 1h; -78 deg C -> 0 deg C;100%
75-16-1

methylmagnesium bromide

93559-82-1

3-fluoro-5H-dibenzocyclohepten-5-one

125025-39-0

3-fluoro-5-methyl-5H-dibenzocyclohepten-5-ol

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 6h; Ambient temperature;100%
75-16-1

methylmagnesium bromide

124098-64-2

6-(benzyloxy)-2,4-dimethylfuro<2,3-b>pyridine-5-carboxaldehyde

124098-67-5

5-(1-hydroxyethyl)-6-(benzyloxy)-2,4-dimethylfuro<2,3-b>pyridine

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether at 0℃; for 0.25h;100%
75-16-1

methylmagnesium bromide

80783-99-9, 124931-15-3, 113474-86-5

N-methoxy-N-methylcinnamamide

1896-62-4

(E)-benzalacetone

Conditions
ConditionsYield
In tetrahydrofuran at 0℃;100%
In tetrahydrofuran; diethyl ether at 0 - 20℃; for 2h;98%
Stage #1: N-methoxy-N-methylcinnamamide With methyl 4-bromocinnamate; triethylsilyl trifluoromethyl sulfonate; triethylphosphine In toluene at 110℃; for 5h; Inert atmosphere;
Stage #2: methylmagnesium bromide In tetrahydrofuran; toluene at -78℃; Inert atmosphere;
Stage #3: With tetrabutyl ammonium fluoride In tetrahydrofuran; toluene for 0.5h; Inert atmosphere;
83%
75-16-1

methylmagnesium bromide

Benzoic acid (2S,3S)-2-formyl-1-(4-methoxy-phenyl)-4-oxo-azetidin-3-yl ester

Benzoic acid (2R,3S)-2-(1-hydroxy-ethyl)-1-(4-methoxy-phenyl)-4-oxo-azetidin-3-yl ester

Conditions
ConditionsYield
In tetrahydrofuran at -45℃;100%
75-16-1

methylmagnesium bromide

134197-98-1

(E)-3-(furan-2-yl)-N-methoxy-N-methylprop-2-enamide

623-15-4

(E)-4-(furan-2-yl)but-3-en-2-one

Conditions
ConditionsYield
In tetrahydrofuran at 0℃;100%
75-16-1

methylmagnesium bromide

134197-97-0

(E)-N-methoxy-N-methyl-3-(thiophen-2-yl)acrylamide

874-83-9, 33603-63-3

(E)-4-(2-thienyl)but-3-en-2-one

Conditions
ConditionsYield
In tetrahydrofuran at 0℃;100%
75-16-1

methylmagnesium bromide

134197-91-4

(1S,3R)-2,2-Dimethyl-3-phenyl-cyclopropanecarboxylic acid methoxy-methyl-amide

134197-90-3

[(1RS,3SR)-2,2-dimethyl-3-phenylcyclopropyl]ethanone

Conditions
ConditionsYield
100%
75-16-1

methylmagnesium bromide

134197-96-9

(E)-N-Methoxy-3-(6-methoxy-naphthalen-2-yl)-N-methyl-acrylamide

127053-22-9

4-(6'-methoxy-2'-naphthyl)-3-buten-2-one

Conditions
ConditionsYield
In tetrahydrofuran at 0℃;100%
75-16-1

methylmagnesium bromide

134197-94-7

(E)-N-Methoxy-N-methyl-3-(3-phenoxy-phenyl)-acrylamide

121488-67-3

(E)-1-(3-Phenoxyphenyl)buten-3-one

Conditions
ConditionsYield
In tetrahydrofuran at 0℃;100%
75-16-1

methylmagnesium bromide

134197-95-8

(E)-3-(4-(benzyloxy)phenyl)-N-methoxy-N-methylacrylamide

75676-91-4

1-(4-benzyloxyphenyl)but-1-en-3-one

Conditions
ConditionsYield
In tetrahydrofuran at 0℃;100%
75-16-1

methylmagnesium bromide

134197-93-6

(E)-N-Methoxy-N-methyl-3-[4-(1-phenyl-ethoxy)-phenyl]-acrylamide

134197-92-5

(E)-4-[4-(1-Phenyl-ethoxy)-phenyl]-but-3-en-2-one

Conditions
ConditionsYield
In tetrahydrofuran at 0℃;100%
75-16-1

methylmagnesium bromide

122421-16-3

2-<(trimethylsilyl)methyl>-2-butenal

141023-16-7

(Z)-3-((trimethylsilyl)methyl)pent-3-en-2-ol

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 0.333333h; Ambient temperature;100%
75-16-1

methylmagnesium bromide

136964-79-9

C26H24O2S

79979-60-5

11-methyl-12-phenyl-9,10-dihydro-9,10-etheno-anthracene

Conditions
ConditionsYield
palladium(II) acetylacetonate In tetrahydrofuran Heating;100%
75-16-1

methylmagnesium bromide

134454-00-5

Methyl (1R,2S)-2-<2-(3-Isopropylphenyl)ethyl>-1-methyl-3-oxo-1-cyclohexanecarboxylate

134365-17-6

Methyl (1R,2S,3R)-1,3-Dimethyl-1-hydroxy-2<2-(3-isopropylphenyl)-ethyl>cyclohexanecarboxylate

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 2h;100%
75-16-1

methylmagnesium bromide

141807-44-5, 126613-06-7, 128544-05-8, 128575-34-8

(+/-)-2,2'-bis(trifluoromethanesulfonyloxy)-1,1-binaphthyl

Conditions
ConditionsYield
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In diethyl ether at 0℃; for 24h; Reflux;100%
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In diethyl ether at 20℃;99%
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In diethyl ether at 20℃; for 1h; Substitution;99%
75-16-1

methylmagnesium bromide

154811-20-8

8-oxabicyclo<3.2.1>oct-6-en-2-one

(1R,2R,5R)-2-Methyl-8-oxa-bicyclo[3.2.1]oct-6-en-2-ol

Conditions
ConditionsYield
In diethyl ether at 0℃;100%
In diethyl ether at 0℃;
1121-60-4

pyridine-2-carbaldehyde

75-16-1

methylmagnesium bromide

Conditions
ConditionsYield
In diethyl ether at 0℃; for 2h;100%
In diethyl ether at 0 - 5℃; for 2h; Inert atmosphere;61%
Yield given;
75-16-1

methylmagnesium bromide

161659-30-9

(3aS,5R,5aR,6aS,9aS,9bS,9cS)-5-Methoxy-1,1,8,8,9c-pentamethyl-decahydro-4,7,9-trioxa-cyclopenta[e]acenaphthylen-6-one

161659-31-0

1,2,3,3aβ,5aβ,6,6aα,9aα,9bα,9c-decahydro-6α-hydroxy-5β-methoxy-1,1,6β,8,8,9cβ-hexamethyl-5H-furo<4',3',2':4,5>naphtho<1,2-d><1,3>dioxolane

Conditions
ConditionsYield
In diethyl ether for 1h; Ambient temperature;100%
75-16-1

methylmagnesium bromide

157396-11-7

7-(4-chlorophenylthio)-6,7-dihydro-1-(phenylsulfonyl)-1H-indol-4(5H)-one

146564-05-8

1-Benzenesulfonyl-7-(4-chloro-phenylsulfanyl)-4-methyl-4,5,6,7-tetrahydro-1H-indol-4-ol

Conditions
ConditionsYield
In tetrahydrofuran for 4h; Ambient temperature;100%
75-16-1

methylmagnesium bromide

161227-56-1

Bis-(1-triisopropylsilanyl-1H-pyrrol-3-yl)-methanone

161227-57-2

C28H50N2Si2

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 2h; Ambient temperature;100%
75-16-1

methylmagnesium bromide

2-Benzyl-6-methyl-1-phenyl-3,4-dihydro-isoquinolinium; iodide

174784-47-5

2-benzyl-1,6-dimethyl-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Conditions
ConditionsYield
In tetrahydrofuran for 1h; Ambient temperature;100%
75-16-1

methylmagnesium bromide

2-Benzyl-1-cyclohexyl-3,4-dihydro-isoquinolinium; bromide

126115-25-1

2-benzyl-1-cyclohexyl-1-methyl-1,2,3,4-tetrahydroisoquinoline

Conditions
ConditionsYield
In tetrahydrofuran for 1h; Ambient temperature;100%
75-16-1

methylmagnesium bromide

(1S,2R,5S)-2-Benzyloxy-1,5-dimethyl-8-oxa-bicyclo[3.2.1]octan-6-one

(1R,2S,5R,6R)-2-Benzyloxy-1,5,6-trimethyl-8-oxa-bicyclo[3.2.1]octan-6-ol

Conditions
ConditionsYield
In diethyl ether100%
75-16-1

methylmagnesium bromide

91103-47-8

N-(tert-butoxycarbonyl)-D-alanine methyl ester

186466-64-8

((R)-2-hydroxy-1,2-dimethyl-propyl)-carbamic acid tert-butyl ester

Conditions
ConditionsYield
Stage #1: methylmagnesium bromide; N-(tert-butoxycarbonyl)-D-alanine methyl ester In tetrahydrofuran at 0 - 20℃; for 16h;
Stage #2: With water In tetrahydrofuran Cooling with ice;
100%
Stage #1: methylmagnesium bromide; N-(tert-butoxycarbonyl)-D-alanine methyl ester In tetrahydrofuran at 0 - 20℃; for 3h;
Stage #2: With water; ammonium chloride In tetrahydrofuran
99%
In tetrahydrofuran; diethyl ether at 0 - 25℃; for 2h;99%
Raw Materials
74-83-9
74-95-3
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    75-16-1

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    Magnesium, bromomethyl-

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    Methylmagnesium bromide CAS NO.75-16-1

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  • Methylmagnesium bromide cas 75-16-1

  • Casno:

    75-16-1

    MSDS/COA Download

    Methylmagnesium bromide cas 75-16-1

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*Required Fields

Chemistry

MF: CH3BrMg
MW: 119.24
density  1.035 g/mL at 25 °C
Fp  77 °F
storage temp.  water-free area
Sensitive  Air & Moisture Sensitive

Toxicity Data With Reference

RTECS  OM3700000

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

May ignite spontaneously in air. A very dangerous fire hazard when exposed to heat or flame; can react vigorously with oxidizing materials. When heated to decomposition it emits acrid smoke and irritating fumes. See also ETHERS, MAGNESIUM COMPOUNDS, and BROMIDES.

Standards and Recommendations

DOT Classification:  4.3; Label: Dangerous When Wet, Flammable Liquid