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Basic Information
| CAS No.: | 762-75-4 |
|---|---|
| Name: | TERT-BUTYL FORMATE |
| Molecular Structure: | |
|
|
|
| Formula: | C5H10 O2 |
| Molecular Weight: | 102.133 |
| Synonyms: | Formicacid, tert-butyl ester (7CI,8CI); tert-Butyl alcohol, formate (6CI);2-Methyl-2-propyl formate; tert-Butyl formate |
| Density: | 0.872 g/mL at 25 °C(lit.) |
| Melting Point: | -93.85°C (estimate) |
| Boiling Point: | 82-83 °C(lit.) |
| Flash Point: | 15 °F |
| Hazard Symbols: |
 F, Xi
|
| Risk Codes: | R11; R36/37; R43 |
| Safety: | 1738871 |
| PSA: | 26.30000 |
| LogP: | 1.59380 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane at 40℃; for 72h; | 94% |
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane for 144h; Ambient temperature; | 92% |
Conditions
| Conditions | Yield |
|---|---|
| With silica triflate In hexane for 0.05h; Heating; | 90% |
| With sulfuric acid; silica gel In hexane for 0.583333h; Heating; | 85% |
| With aminopropylated mesoporous SBA-15 silica at 40℃; for 0.5h; Neat (no solvent); chemoselective reaction; | 80% |
Conditions
| Conditions | Yield |
|---|---|
| 89% | |
| 89% | |
| 89% |
- 24424-99-5
di-tert-butyl dicarbonate
- 762-75-4
tert-butyl formate
Conditions
| Conditions | Yield |
|---|---|
| In dichloromethane | 75.8% |
- 507-20-0
tertiary butyl chloride
- 124-38-9
carbon dioxide
A
- 762-75-4
tert-butyl formate
B
- 75-65-0
tert-butyl alcohol
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; sodium hydrogencarbonate; {W(CO)5Cl}(1-) In tetrahydrofuran at 150℃; under 80 - 85 Torr; for 24h; | A 73.3% B 26.7% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With [bis({2‐[bis(propan‐2‐yl)phosphanyl]ethyl})amine](borohydride)(carbonyl)(hydride)iron(II); methacrylic acid methyl ester In toluene at 140℃; under 13689.1 Torr; for 8h; Reagent/catalyst; Autoclave; Inert atmosphere; | 71% |
- 24424-99-5
di-tert-butyl dicarbonate
- 762-75-4
tert-butyl formate
Conditions
| Conditions | Yield |
|---|---|
| With N-ethyl-N,N-diisopropylamine In 1,4-dioxane; water | 62% |
| In 1,4-dioxane; water | |
| With sodium hydroxide In 1,4-dioxane |
- 865-47-4
potassium tert-butylate
- 87442-43-1
dimethyl 2-(10-methyl-9,10-dihydroacridin-9-yl)malonate
A
- 719-54-0
10-methyl-9, 10-dihydro-9-acridinone
B
- 762-75-4
tert-butyl formate
Conditions
| Conditions | Yield |
|---|---|
| With oxygen In dimethyl sulfoxide at 70℃; | A 50.4% B n/a |
...Expand
- 87442-43-1
dimethyl 2-(10-methyl-9,10-dihydroacridin-9-yl)malonate
A
- 719-54-0
10-methyl-9, 10-dihydro-9-acridinone
B
- 762-75-4
tert-butyl formate
Conditions
| Conditions | Yield |
|---|---|
| With oxygen In dimethyl sulfoxide at 70℃; | A 50.4% B n/a |
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