CAS No.89-55-4,5-Bromosalicylic acid Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	89-55-4
Name:	5-Bromosalicylic acid
Article Data:	72

Formula:	C₇H₅BrO₃
Molecular Weight:	217.019
Synonyms:	Salicylicacid, 5-bromo- (6CI,8CI);2-Hydroxy-5-bromobenzoic acid;5-Bromo-2-hydroxybenzoic acid;NSC 3981;NSC 52393;
EINECS:	201-917-0
Density:	1.861 g/cm³
Melting Point:	162-166 °C
Boiling Point:	338.1 °C at 760 mmHg
Flash Point:	158.3 °C
Solubility:	Soluble in water
Appearance:	white to slightly beige powder
Hazard Symbols:	Xi
Risk Codes:	36/37/38
Safety:	37/39-26-36
PSA:	57.53000
LogP:	1.85290

Synthetic route

: 69-72-7
salicylic acid

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
With tetrapropylammonium nonabromide In dichloromethane at 23℃; for 0.5h; Inert atmosphere;	95%
With sodium vanadate; aluminum tri-bromide; tetrabutylammomium bromide; oxygen In 1,4-dioxane; water at 80℃; for 8h; Reagent/catalyst; Solvent; Temperature;	93.1%
With 1-butyl-3-methylpyridinium tribromide at 20℃; for 1h;	89%

: 1761-61-1
5-bromosalicyclaldehyde

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
With sodium chlorite; sodium methylate In dimethyl sulfoxide	84%

: 21740-00-1
5-bromo-2-iodo-benzoic acid

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
With copper(I) oxide; 1-D-O-Methyl-chiro-inositol; sodium hydroxide In water at 100℃; for 6h;	77%

: 82486-43-9
2-hydroxy-5-bromobenzaldehyde oxime

A: 89-55-4
5-bromosalicyclic acid

B: 1761-61-1
5-bromosalicyclaldehyde

Conditions

Conditions	Yield
With calcium hypochlorite; montmorillonite K-10 In chloroform at 20℃; for 4h;	A 2.5% B 69%

: 4-bromo-2-propionylphenylmethylphenylcarbamate

A: 5827-78-1
N-methyl-N-phenylpropanamide

B: 89-55-4
5-bromosalicyclic acid

C: 17764-93-1
5-bromo-2-hydroxypropiophenone

Conditions

Conditions	Yield
With water; sodium hydride In tetrahydrofuran for 24h; Reflux;	A 60% B 43% C n/a

...Expand

: 56-23-5
tetrachloromethane

: 106-41-2
4-bromo-phenol

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
With sodium hydroxide

: 109-72-8, 29786-93-4
n-butyllithium

: 60-29-7
diethyl ether

: 615-58-7
2,4-dibromophenol

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
anschliessend Behandeln mit festem Kohlendioxid;

...Expand

: 615-58-7
2,4-dibromophenol

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
With n-butyllithium; diethyl ether anschliessendes Behandeln mit CO2;

: 10268-63-0
phenyl 5-bromo-2-hydroxybenzoate

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
bei der Verseifung;

: 4068-76-2
5-bromo-2-hydroxy-benzoic acid methyl ester

: 89-55-4
5-bromosalicyclic acid

Conditions

Conditions	Yield
With sodium hydroxide

Raw Materials

7732-18-5

54-21-7

106-41-2

109-72-8

118-61-6

Downstream Products

323-87-5

Total:75 Page 1 of 2 1 2 Next>>

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Chemistry

5-Bromosalicylic acid(89-55-4) is the chemical compound with the formula C₇H₅BrO₃.Its molar weight is 217.02g/mol.
5-Bromosalicylic acid(89-55-4) is also named 2-Hydroxy-5-bromobenzoic acid;3-bromo-6-hydroxy-benzoicaci;5-bromo-2-hydroxy-benzoicaci;5-bromo-salicylicaci;Benzoic acid, 3-bromo-6-hydroxy-;Benzoic acid, 5-bromo-2-hydroxy-;Benzoicacid,5-bromo-2-hydroxy-;Salicylic acid, 5-bromo-.
Melting Point: 162-166 ^oC
Boiling Point: 338.1 ^oC at 760 mmHg
Flash Point: 158.3 ^oC
Water Solubility: Soluble
Index of Refraction: 1.654
Molar Refractivity: 42.75 cm³
Molar Volume: 116.5 cm³
Surface Tension: 68.1 dyne/cm
Density: 1.861 g/cm³
Enthalpy of Vaporization: 61.36 kJ/mol
Vapour Pressure: 3.93E-05 mmHg at 25 ^oC
The chemical structure of 5-Bromosalicylic acid(89-55-4) is

Uses

5-Bromosalicylic acid(89-55-4) is used as organic synthesis.

Toxicity Data With Reference

ivn-mus LD50:100 mg/kg

CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#04478 .

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intravenous route. When heated to decomposition it emits toxic fumes of Br⁻.
Hazard Codes:

Xi
Risk Statements: 36/37/38
36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 37/39-26-36
37/39: Wear suitable gloves and eye/face protection
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
RTECS: VO1850000.

Specification

5-Bromosalicylic acid(89-55-4)The extinguishing agents of 5-Bromosalicylic acid(89-55-4) is dry powder, carbon dioxide, water mist.