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993-07-7

Basic Information
CAS No.: 993-07-7
Name: TRIMETHYLSILANE
Article Data: 135
Molecular Structure:
Molecular Structure of 993-07-7 (TRIMETHYLSILANE)
Formula: C3H10Si
Molecular Weight: 74.1979
Synonyms: 2-Methyl-2-silapropane;Dow Corning 9-5170;Trimethylsilyl hydride;
EINECS: 213-603-0
Density: 0.638 g/cm3
Melting Point: -135,9 °C
Boiling Point: 1.67 °C at 760 mmHg
Flash Point: -72.532 °C
Solubility: 1.4g/L at 20℃
Risk Codes: 12-36/37/38
Safety: 9-16-26-33
PSA: 0.00000
LogP: 1.10290
Synthetic route
16853-85-3

lithium aluminium tetrahydride

75-77-4

chloro-trimethyl-silane

993-07-7

trimethylsilan

Conditions
ConditionsYield
aluminum (III) chloride; lithium chloride In xylene at 80℃; for 0.166667h; Product distribution / selectivity;95.4%
In toluene at 80℃; for 0.166667h; Product distribution / selectivity;92.5%
lithium tetrachloroaluminate In toluene at 80℃; for 0.166667h; Product distribution / selectivity;92.7%
6651-36-1

1-(Trimethylsilyloxy)cyclohexene

A

993-07-7

trimethylsilan

B

108-94-1

cyclohexanone

Conditions
ConditionsYield
With hydrogen; [RuCl(η2-H2)(dppe)2]OTf In 1,2-dichloro-ethane at 50℃; under 760 Torr; for 48h; Product distribution; Further Variations:; Catalysts;A n/a
B 95%
With hydrogen; [RuCl(dppe)2]OTf In benzene-d6 at 50℃; for 3h; Hydrogenolysis; Title compound not separated from byproducts;
27607-77-8

trimethylsilyl trifluoromethanesulfonate

993-07-7

trimethylsilan

Conditions
ConditionsYield
With C35H37IrN2P(1+)*C24BF20(1-); hydrogen; N-ethyl-N,N-diisopropylamine; triphenylphosphine In (2)H8-toluene at 20℃; under 760.051 Torr; for 4.5h;94%
With [N-[4-(dimethylamino)phenyl]-2-pyridinecarboxamidato](pentamethylcyclopentadienyl)iridium trifluorometanesulfonate; hydrogen; N-ethyl-N,N-diisopropylamine In benzene-d6 at -196 - 60℃; under 3040.2 Torr; for 48h;95 %Spectr.
With 1,4-bis-(trimethylsilyl)benzene; [N-[4-(dimethylamino)phenyl]-2-pyridinecarboxamidato](pentamethylcyclopentadienyl)iridium trifluorometanesulfonate; hydrogen; N-ethyl-N,N-diisopropylamine In benzene-d6 at 60℃; under 3040.2 Torr; for 48h; Reagent/catalyst;95 %Spectr.
With [Ru(H)2CO(HN(CH2CH2P(iPr)2)2)]; hydrogen; triethylamine In benzene-d6 at 20℃; under 3000.3 Torr; for 18h; Catalytic behavior; Pressure;85 %Spectr.
75-77-4

chloro-trimethyl-silane

993-07-7

trimethylsilan

Conditions
ConditionsYield
With lithium aluminium tetrahydride; calcium hydride In diethylene glycol dimethyl ether for 11h; Inert atmosphere; Reflux;92%
With lithium aluminium tetrahydride In toluene at 80℃; for 0.916667h; Inert atmosphere;82%
With lithium aluminium tetrahydride In hexane at 40℃; for 3h; Irradiation; ultrasonic irradiation;80%
83268-94-4

C10H26OSi3

A

6224-91-5

trimethyl(prop-1-ynyl)silane

B

993-07-7

trimethylsilan

C

1825-61-2

Methoxytrimethylsilane

D

754-05-2

ethenyltrimethylsilane

Conditions
ConditionsYield
at 650℃; under 0.0001 Torr;A 18%
B n/a
C 87%
D 28%
814-98-2

1,1,2,2-tetramethyldisilane

A

75-77-4

chloro-trimethyl-silane

B

1066-35-9

dimethylmonochlorosilane

C

1111-74-6

dimethylsilane

D

993-07-7

trimethylsilan

Conditions
ConditionsYield
With tetra-n-butylphosphonium chloride at 180℃; for 17h; Sealed tube;A 2%
B 4%
C 87%
D 7%
1560-28-7

pentamethylchlorodisilane

A

75-77-4

chloro-trimethyl-silane

B

993-07-7

trimethylsilan

Conditions
ConditionsYield
With 2-methylimidazole; tetra-n-butylphosphonium chloride at 175℃; for 89h; Sealed tube;A 85%
B 11%
766-77-8

Dimethylphenylsilane

17961-91-0

3-dimethylaminophenyl-trimethylsilane

A

993-07-7

trimethylsilan

B

3-(dimethyl(phenyl)silyl)-N,N-dimethylaniline

Conditions
ConditionsYield
With tris(pentafluorophenyl)borate In chlorobenzene at 100℃; for 24h; Mechanism; Glovebox; Inert atmosphere; chemoselective reaction;A n/a
B 81%

3-(dimethylsilyl)-N,N-dimethylaniline

A

993-07-7

trimethylsilan

B

3,3′-(dimethylsilanediyl)-bis(N,N-dimethylaniline)

Conditions
ConditionsYield
With trimethylphenylsilane; tris(pentafluorophenyl)borate In chlorobenzene at 100℃; for 24h; Mechanism; Glovebox; chemoselective reaction;A n/a
B 78%
83268-89-7

2-cyclopropyl-2-methoxyhexamethyltrisilane

A

6224-91-5

trimethyl(prop-1-ynyl)silane

B

993-07-7

trimethylsilan

C

1825-61-2

Methoxytrimethylsilane

D

754-05-2

ethenyltrimethylsilane

Conditions
ConditionsYield
at 590℃; under 0.0001 Torr;A 18%
B n/a
C 72%
D 27%
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