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1001-53-2

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1001-53-2 Usage

Chemical Properties

White to yellow crystalline solid

Uses

N-(2-Aminoethyl)acetamide may be used in the preparation of mixed two-component monolayers on glassy carbon. It may be used in the synthesis of lysidine.

General Description

N-(2-Aminoethyl)acetamide is an organic building block.

Purification Methods

The acetyl-diamine has been fractionated under reduced pressure and fraction b 125-130o/5mm was refractionated, fraction b 132-135o/4mm was collected and solidified. It is a low melting hygroscopic solid which can be recrystallised from dioxane/Et2O. It is soluble in H2O, Et2O and *C6H6. The p-toluenesulfonate salt can be recrystallised from EtOH/EtOAc (1:8), has m 125-126o but the free base cannot be recovered from it by basifying and extracting with CH2Cl2. The picrate has m 175o (from EtOH) [Aspinall J Am Chem Soc 63 853 1941, Hall J Am Chem Soc 78 2570 1956]. [Beilstein 4 IV 1193.]

Check Digit Verification of cas no

The CAS Registry Mumber 1001-53-2 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 1,0,0 and 1 respectively; the second part has 2 digits, 5 and 3 respectively.
Calculate Digit Verification of CAS Registry Number 1001-53:
(6*1)+(5*0)+(4*0)+(3*1)+(2*5)+(1*3)=22
22 % 10 = 2
So 1001-53-2 is a valid CAS Registry Number.
InChI:InChI=1/C4H10N2O/c1-4(7)6-3-2-5/h2-3,5H2,1H3,(H,6,7)

1001-53-2 Well-known Company Product Price

  • Brand
  • (Code)Product description
  • CAS number
  • Packaging
  • Price
  • Detail
  • Alfa Aesar

  • (L13398)  N-Acetylethylenediamine, tech. 90%   

  • 1001-53-2

  • 5g

  • 752.0CNY

  • Detail
  • Alfa Aesar

  • (L13398)  N-Acetylethylenediamine, tech. 90%   

  • 1001-53-2

  • 25g

  • 2562.0CNY

  • Detail
  • Aldrich

  • (397261)  N-(2-Aminoethyl)acetamide  technical grade, 90%

  • 1001-53-2

  • 397261-5G

  • 410.67CNY

  • Detail
  • Aldrich

  • (397261)  N-(2-Aminoethyl)acetamide  technical grade, 90%

  • 1001-53-2

  • 397261-25G

  • 1,554.93CNY

  • Detail

1001-53-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name N-(2-Aminoethyl)acetamide

1.2 Other means of identification

Product number -
Other names Acetamide, N-(2-aminoethyl)-

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1001-53-2 SDS

1001-53-2Relevant articles and documents

-

Haake,Watson

, p. 4063,4064 (1970)

-

Synthesis and characterization of polyamidoamine dendrimers surface-functionalized with bromotricarbonylpyridyliminerhenium(I) units

Zhao, Xinxin,Yan, Yaw-Kai,Chu, Chit-Kay

, p. 5540 - 5546 (2006)

A novel type of rhenium-containing dendrimers has been prepared and characterized. A series of Schiff base-terminated PAMAM dendrimers were prepared by condensing the terminal amine groups of PAMAM dendrimers with pyridine-2-carboxaldehyde. Complete condensation of the terminal amines was confirmed by 1H NMR spectroscopy. Bromotricarbonylrhenium(I) moieties were introduced onto the surface of these modified PAMAM derivatives by refluxing with bromopentacarbonylrhenium(I). These complexes had been characterized by a variety of analytical and spectroscopic techniques and their IR, NMR, and mass spectra discussed. The crystal structure of the model compound [(CH3CONHCH2CH2N{double bond, long}CH{single bond}Py)ReBr(CO)3] confirms a facial configuration of the three carbonyl ligands. UV-Vis absorption spectroscopy suggests that the {Re(CO)3} moieties are quite far apart even in the second generation PAMAM dendrimers and do not interact with one another. In fact, the intensity of the metal-to-ligand (dπ-pπ*) charge-transfer is a linear function of the number of {Re(CO)3} chromophores.

Structural analysis of ATP analogues compatible with kinase-catalyzed labeling

Suwal, Sujit,Senevirathne, Chamara,Garre, Satish,Pflum, Mary Kay H.

, p. 2386 - 2391 (2012)

Kinase-catalyzed protein phosphorylation is an important biochemical process involved in cellular functions. We recently discovered that kinases promiscuously accept γ-modified ATP analogues as cosubstrates and used several ATP analogues as tools for stud

The mechanisms of the formation of by-products in the catalytic synthesis of C-alkylimidazoles from diamines and carboxylic acids

Gitis, K. M.,Raevskaya, N. I.,Isagulyants, G. V.

, p. 895 - 898 (1993)

The formation of 1-ethyl-2-methylimidazole (1-Et-2-MI) and 1-ethyl-2-methylimidazoline (1-Et-2-MIN), intermediates in the synthesis of 2-methylimidazole (2-MI) from ethylenediamine (EDA) and AcOH in the presence of a platinum-on-alumina catalyst, was studied.Using CH3(14)COOH the incorporation of two acetate units into 1-Et-2-MI and 1-Et-2-MIN molecules was demonstrated.The same products were also obtained on dehydrogenation of 2-methylimidazoline (2-MIN) under mild conditions (220-230 deg C).A part of the latter is transformed to N-ethyl ethylendiamine (EEDA) and EDA.These facts indicate that both 1-Et-2-MI and 1-Et-2-MIN result from hydrogenolysis of the imidazoline ring with subsequent ethylation.A reverse reaction, the C5-cyclization of EEDA, was also observed.The formation of 2-MI is favored by increasing temperature.

WDR5 INHIBITORS AND MODULATORS

-

Paragraph 00326; 00327, (2021/05/15)

Isoquinolmone compounds and derivatives inhibit WDR5 and associated protein-protein interactions, and the compounds and their pharmaceutical compositions are useful for treating disorders and conditions in a subject, such as cancer cell proliferation.

Simple and Versatile Laboratory Scale CSTR for Multiphasic Continuous-Flow Chemistry and Long Residence Times

Chapman, Michael R.,Kwan, Maria H. T.,King, Georgina,Jolley, Katherine E.,Hussain, Mariam,Hussain, Shahed,Salama, Ibrahim E.,González Nino, Carlos,Thompson, Lisa A.,Bayana, Mary E.,Clayton, Adam D.,Nguyen, Bao N.,Turner, Nicholas J.,Kapur, Nikil,Blacker, A. John

, p. 1294 - 1301 (2017/09/23)

A universal multistage cascade CSTR has been developed that is suitable for a wide range of continuous-flow processes. Coined by our group the "Freactor" (free-to-access reactor), the new reactor integrates the efficiency of pipe-flow processing with the advanced mixing of a CSTR, delivering a general "plug-and-play" reactor platform which is well-suited to multiphasic continuous-flow chemistry. Importantly, the reactor geometry is easily customized to accommodate reactions requiring long residence times (≥3 h tested).

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