High-nuclearity silver ethynide cluster encapsulating a template hexafluorosilicate ion
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Add time:07/26/2019 Source:sciencedirect.com
A novel high-nuclearity silver(I) ethynide cluster complex, namely {SiF6@Ag24(CCtBu)20}·SiF6, has been isolated from the reaction between AgBF4 and tBuCCAg in a glass beaker. Single-crystal X-ray analysis showed that an in situ generated hexafluorosilicate template anion occupies the central cavity of the cationic polyhedral Ag24 cluster, which is consolidated by peripheral tert-butyl ethynide groups and inter-cluster hexafluorosilicate ions.
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