The thermal decomposition of metal complexes—XIII: Some tetramminepalladium(II) complexes

Add time:08/27/2019    Source:sciencedirect.com

The thermal dissociation of the palladium(II) tetrammine-complexes, [Pd(NH3)4]X (where X is 2Cl, 2Br, 2I, 2NO3, and SO4), was studied by thermogravimetry, DTA, GE, and by analysis of the pyrolysis products. The complexes, except for the nitrate and sulphate, dissociated to give the trans-diammine-complexes, [Pd(NH3)2X]. The diammine-iodide and bromide complexes dissociated to give the corresponding anhydrous metal halides, PdX2. The stoicheiometry for the thermal dissociation of the [Pd(NH3)2X2] complexes, where X was Cl, Br, and I, was determined.

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