N-(2-Methyl-5-tert-butyl-phenyl)-N-tert-butyl-nitroxide, a new thermally stable nitroxide
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Add time:09/03/2019 Source:sciencedirect.com
Quenching with tert-butyl nitroso 2-lithio-4-tert-butyl toluene prepared by an exchange reaction with t-butyl-lithium, followed by acidic hydrolysis furnishes in good yields the corresponding aromatic hydroxylamine whose oxidation affords the nitroxide, N-(2-methyl-5-tert-butyl-phenyl)-N-tert-butyl-nitroxide. This nitroxide did not undergo decomposition after heating 17 h in solution at 105 °C.
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