Silphos [PCl3−n(SiO2)n]: a heterogeneous phosphine reagent for formylation and acetylation of alcohols and amines with ethyl formate and acetate
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Add time:09/06/2019 Source:sciencedirect.com
Alcohols and amines are formylated and acetylated in the presence of Silphos [PCl3−n(SiO2)n] in ethyl formate and ethyl acetate in high to excellent yields. This procedure provides a method to separate the product by a simple filtration.
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