Synthesis of 1,2-aminoazides. Conversion to unsymmetrical vicinal diamines by catalytic hydrogenation or reductive alkylation with Dichloroborane (cas 13701-67-2)s.
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Add time:10/01/2019 Source:sciencedirect.com
1,2-aminoazides are easily prepared from 1,2-amino alcohols. Catalytic hydrogenation in the presence of palladium on charcoal or reductive alkylation with dichloroboranes afford with good yields unsymmetrically substituted vicinal diamines.
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