A new preparation of 4-(BOC-aminoacyloxymethyl)phenylacetic acids for solid-phase peptide synthesis
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Add time:09/08/2019 Source:sciencedirect.com
A new preparation of 4-(BOC-aminoacyloxymethyl)phenylacetic acids 1, consisting of an esterification of the corresponding BOC-amino acids 2 with 4-(bromomethyl)phenethyl alcohol 3, followed by a Collins oxidation and an oxidation with sodium chlorite is described. The overall yields range from 58 to 69%.
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