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Conditions | Yield |
---|---|
In 1,4-dioxane; water at 19 - 44℃; Thermodynamic data; Kinetics; Rate constant; conductometrical measurements, different ratios dioxane/water, other temperatures, hydrolysis constants, ΔS(excit.), ΔH(excit.), isotopical kinetic effects; | 98.6% |
With amide; HY zeolite In water at 180℃; for 0.0666667h; microwave irradiation; | 97% |
With water at 20℃; |
2-<5'-(Dimethylamino)-4',4'-dimethyl-4'H-imidazol-2'-yl>-2-ethylbutanamid
A
5-(Dimethylamino)-2-(1-ethylpropyl)-4,4-dimethyl-4H-imidazol
B
isocyanuric acid
Conditions | Yield |
---|---|
at 120℃; | A 95% B n/a |
at 120℃; Yields of byproduct given; |
2-<5'-(Dimethylamino)-4',4'-dimethyl-4'H-imidazol-2'-yl>-2-phenylpentanamid
A
5-(Dimethylamino)-4,4-dimethyl-2-(1-phenylbutyl)-4H-imidazol
B
isocyanuric acid
Conditions | Yield |
---|---|
In 1,1,2,2-tetrachloroethylene for 72h; Heating; | A 93% B n/a |
In 1,1,2,2-tetrachloroethylene Heating; Yields of byproduct given; |
Conditions | Yield |
---|---|
With water; triethylamine In acetone at 0 - 5℃; for 4h; | 93% |
Conditions | Yield |
---|---|
at 200℃; Temperature; Inert atmosphere; | 92.55% |
trichloroisocyanuric acid
thiophenol
A
isocyanuric acid
B
diphenyldisulfane
Conditions | Yield |
---|---|
With pyridine; water; benzoic acid In dichloromethane; acetonitrile at 40℃; | A n/a B 91% |
2-<5'-(Dimethylamino)-4',4'-dimethyl-4'H-imidazol-2'-yl>-2-phenylbutanamid
A
5-(Dimethylamino)-4,4-dimethyl-2-(1-phenylpropyl)-4H-imidazol
B
isocyanuric acid
Conditions | Yield |
---|---|
at 153℃; | A 90% B n/a |
at 153℃; Yields of byproduct given; |
trichloroisocyanuric acid
para-thiocresol
A
di(p-tolyl) disulfide
B
isocyanuric acid
Conditions | Yield |
---|---|
With pyridine; water; benzoic acid In dichloromethane; acetonitrile at 40℃; | A 89% B n/a |
Conditions | Yield |
---|---|
In kerosene at 190℃; | 88.9% |
2,4-bis(3,5-dimethyl-1H-pyrazol-1-yl)-6-methoxy-1,3,5-triazine
A
3,5-dimethyl-1H-pyrazole
B
isocyanuric acid
Conditions | Yield |
---|---|
With hydrogenchloride; water for 2h; Reflux; | A 72% B 86% |
1. | eye-rbt 500 mg/24H MLD | 28ZPAK Sbornik Vysledku Toxixologickeho Vysetreni Latek A Pripravku Marhold, J.V.,Institut Pro Vychovu Vedoucicn Pracovniku Chemickeho Prumyclu Praha,Czechoslovakia.: 1972,152. | ||
2. | eye-rbt 20 mg/24H rns MLD | MONS** Monsanto Co. Toxicity Information .(Monsanto Industrial Chemicals Co.,Wilmington, DE.: ) | ||
3. | orl-rat LD50:7700 mg/kg | ZKMAAX Zhurnal Eksperimental’noi i Klinicheskoi Meditsiny. 25 (1985),345. | ||
4. | orl-mus LD50:3400 mg/kg | ZKMAAX Zhurnal Eksperimental’noi i Klinicheskoi Meditsiny. 25 (1985),345. |
Hazard Codes : Xi (Irritant)
Risk Statements :
R36-36/37/38 (Irritating to the eyes ;Irritating to eyes, respiratory system and skin)
Safety Statements :
S26-37/39 (In case of contact with eyes, rinse immediately with plenty of water and seek medical advice ;Wear suitable gloves and eye/face protection)
RIDADR : UN 3389 6.1/PG 1