Bulletin of the Chemical Society of Japan p. 4369 - 4376 (1987)
Update date:2022-08-04
Topics:
Inouye, Yoshinobu
Kojima, Tsutomu
Owada, Jun
Kakisawa, Hiroshi
Bicyclo<3.3.1>nonane-2,4-dione and 7-endo-benzyloxy-9-methylenebicyclo<3.3.1>nonane-2,4-dione were prepared starting from bicyclo<3.3.1>nonan-2-one and 7-endo-benzyloxybicyclo<3.3.1>nonane-2,9-dione, respectively.The key reaction was the NCS oxidation of the 2,2-ethylenedioxy-4-phenylthiobicyclo<3.3.1>nonanes, derived from the corresponding bicyclo<3.3.1>non-3-en-2-ones.
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